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American Environmental Network WORK ORDER. 9709415 QUALITY CONTROL REPORT PAGE QR-6 ANALYSIS Volatile GC/MS MATRIX Sall/Bulk METHOD BLANK SAMPLES --- - -- ---- --- -- - - --- -- --- -- -- --------------- - -- --- --- --- --------------- --- ------- --- ---- - SAMPLE TYPE Blank Method/Media blank LAB ID BLNK 1014 INSTR RUN GCMS13\971014000000/1/ INSTRUMENT HP mass spec for Volatiles PREPARED J BATCH ID MS13SIO1497 UNITS ug/kg ANALYZED 10/14/97 DILUTION 1 00 METHOD REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) trans 1 4 Dichloro-2 buten NO cis 1 3-Dichloropropene ND trans-1,3 Dichloropropene ND 2-Hexanone ND Methyl Iodide ND 4 Methyl 2 pentanone ND Vinyl Acetate ND 2 Chloroethyl Vinyl Ether NO LABORATORY CONTROL SAMPLES - - - -- --- --- --- ------ - -- -------- - SAMPLE TYPE Laboratory Control Spike LAB ID LCS 1014 INSTR RUN GCMS13\971014000000/2/1 INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13SIO1497 UNITS ug/kg ANALYZED 10/14/97 DILUTION 50 0 METHOD ' REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) • 1 2 DCA d4 (surr) 117 108 100 117 60 140 Toluene-d8 (surr) 112 98 7 100 112 60 140 p BFB (surr) 121 101 100 121 60 140 1 1 Dichloroethene 2860 NO 2500 114 4 40 140 Benzene 2840 ND 2500 113 6 60 140 Trichloroethene 2570 ND 2500 106 8 60 140 Toluene 3050 ND 2500 122 0 60 140 Chlorobenzene 3380 ND 2500 135 2 60 140 SAMPLE SURROGATES SAMPLE TYPE Sample-Client LAB ID 9709415 03A INSTR RUN GCMS13\971014000000/31 INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13S101497 UNITS ug/kg ANALYZED 10/14/97 DILUTION 1000 METH00 REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPO ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) 1 2 OCA d4 (surr) D 5000 0 1 60 140 Toluene-d8 (surr) D 5000 0 1 60 140 p BFB (surr) D 5000 0 ► 60 140 i