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Report Number 31947 QC Report Matrix Spike/Matrix Spike Duplicate Date 3114103 ` Project Name Barnes Trucking Project Number ZB178C Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Anel zed Recov Recov Diff Limit Limit Benzene 32023-02 89 39 2 388 113 114 ug/L EPA 8260B 3110103 613 641 452 70-130 25 Toluene 32023-02 063 39 2 388 35 9 358 ug/L EPA 8260B 3110103 898 906 0 814 70-130 25 Tert-Butanol 32023-02 160 196 194 343 341 ug/L EPA 8260B 3110103 925 927 0181 70-130 25 Methyl-t-Butyl Ether 32023-02 270 392 388 296 294 ug/L EPA 8260B 3110103 564 502 117 70-130 25 Benzene 31959-02 <0 50 400 400 406 404 ug/L EPA 82606 318103 101 101 0 420 70-130 25 Toluene 31959-02 <0 50 400 400 376 375 ug/L EPA 8260E 318103 940 938 0160 70-130 25 Tert-Butanol 31959-02 <50 200 200 204 205 ug/L EPA 8260B 318103 102 102 0 616 70-130 25 Methyl-t-Butyl Ether 31959-02 <0 50 400 400 419 41 7 ug/L EPA 8260B 318103 105 104 0 431 70-130 25 Benzene 31947-03 <0 50 400 400 435 428 ug/L EPA 8260B 318103 109 107 155 70-130 25 Toluene 31947-03 <0 50 400 400 39 2 389 ug/L EPA 8260E 318103 981 974 0 742 70-130 25 Tert-Butanol 31947-03 <5 0 200 200 191 198 ug/L EPA 8260E 318103 956 990 341 70-130 25 Methyl-t-Butyl Ether 31947-03 <0 50 400 400 34 3 340 ug/L EPA 82606 318103 856 850 0 821 70-130 25 Benzene 32000-03 <0 50 400 40 0 415 406 ug/L EPA 8260B 3110103 104 102 221 70-130 25 Toluene 32000-03 <0 50 400 400 411 403 ug/L EPA 82608 3110103 103 101 204 70-130 25 Tert-Butanol 32000-03 <5 0 200 200 217 214 ug/L EPA 8260B 3110103 108 107 131 70-130 25 Methyl-t-Butyl Ether 32000-03 <0 50 400 400 363 405 ug/L EPA 82608 3110103 908 101 108 70-130 25 KIFF ANALYTICAL, LLC Approved By J�e1 Koff 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800 U