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May .20 2002 4 57PM No 0027 P 7/13 <br /> Entech Analytical Labs, Inc. <br /> 3334 Victor Court • Santa Clara, CA 95054 - (408) 588-0200 • Fax (408) 588-0201 <br /> Clearwater Croup,Inc. Date 05/20/02 <br /> Date Received 05/15/02 <br /> 229 Tewksbury Avenue Project Narne ZB178C <br /> Point Richmond,CA. 94801. Project Number <br /> Attu Adam Newman PO Number ZB178C <br /> Sampled By Scott Robertson <br /> Certified Aunlytilcal Report <br /> Order ID: 29994 Lab Sample ID 29994-005 Client Sample ID: MW513 <br /> Sample Time. 155 PM Sample Date- 05/10/02 Matrix: Liquid <br /> Parameter Result Flag OF PQL DLR Units fYtraet QR Amalyels QC);etch 1D Method <br /> Date Vats <br /> Benzene 1500 50 05 25 RZ/L N/A 05/16/02 WMS31561 EPA 8260E <br /> Toluene 320 50 05 25 µg/L N/A. 05/16/02 WMS31561 EPA 82608 <br /> Ethyl Benzene 300 50 05 25 Ag/1- N/A Ono= WMS31561 EPA 8260E <br /> xylcucs'Total 560 5o 1 50 118/L N/A 05/16/02 WMS31561 EPA 8260B <br /> surrogate Surrogate Recovery Control Lauuts{%] <br /> a-Bromotluorobenzene 1030 65 135 <br /> Drbromofluoromethane 1034 57 - 156 <br /> Toluene-d8 1132 77 150 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> Methyl-t-butyl Ether ND 50 5 250 gg/L NIA. 05/16/02 WMS31561 EPA 8260B <br /> Surrogate Surrogate Recovery Control Limas{%) <br /> 4-Broznofluorobenzene 1030 73 151 <br /> Dibrosnofluorornethane 1034 57 - 156 <br /> Tof�ne d8 <br /> 1132 77 - 150 <br /> Parameter Remit Flag OF T'Qx. DLR Units Extraction Analysis QC Batch W Method <br /> nate Date <br /> TPH as Gasoline 8I00 50 50 2500 µ8/J- N/A 05/16/02 WMS31561 oc-ms <br /> Surrogate Surrogate Recovery Control IAmits(%) <br /> 4-Bromofluorobenzene 1030 65 - 135 <br /> Drbrornofluoromethane 1034 57 - 156 <br /> Toluene-d8 1132 77 - 150 <br /> DF=Dilution Factor ND=Nat Detected ALR=Detection Lrmat Reported PQL=Practical Qwwwatton Limit <br /> Analysts performed by Enrech Analytical Labs,Inc (CA.EW#2346) <br /> 9Pattiandro , QA/QC Manager Environmental AnalYSIS Since 1983 <br />