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I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell com E-mail main@mccampbell com <br />' Ad Date Sampled 04/24/98 <br /> Advanced GeoEnvironmental Client Project ID #95-0184, Larry's Auto <br />' 4005 North Wilson Way Date Received 04/28/98 <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 04/29-04/30/98 <br />' Client P O Date Analyzed 04/29-04/30/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 88591 <br /> Client ID VW5B/4-24-98 <br /> Matrix W <br />' Compound Concentration* Compound Concentration* <br /> Acetone' ND<540 Ethylbenzene 4300 <br /> Benzene 22,000 Hexachlorobutadiene ND<85 <br />' Bromobenzene ND<85 lodomethane ND<85 <br /> Bromochloromethane ND<85 Isopropylbenzene 130 <br /> Bromodichloromethane ND<85 p-Isoprop)I toluene ND<85 <br /> Bromoform ND<85 Methyl butyl ketone' ' ND<85 <br />' Bromometbane ND<85 Nleth,,lene Chloride"' ND<85 <br /> n Butyl benzene ND<85 Methyl eth)I ketone' ND<85 <br /> sec-Butyl benzene ND<85 Methyl isobutyl ketoneND<85 <br /> tert-Butyl benzene ND<85 Methyl reit-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<85 Naphthalene 650 <br /> Carbon Tetrachloride N13<85 ii-Propyl benzene 310 <br /> Chlorobenzene ND<85 St)iene' ND<85 <br /> Chloroethane ND<85 1,10 2-Teti achIorocthane ND<85 <br />' 2-Chloroethyl Vinyl Ether"' ND<85 1,1 2 2-Tetrachloroethane ND<85 <br /> Chloroform ND<85 Tetrachloroethene ND<85 <br /> Chloromethane ND<85 Toluene' 47,000 <br /> 2 Chlorotoluene ND<85 1,2,3 Trichloiobenzene ND<85 <br />' 4-Chloiotoluene ND<85 1 2,4-Trichloiobenzene ND<85 <br /> Dibroinochloromethane ND<85 1,1 l-Trichloroethane ND<85 <br /> 12-Dibromo-3-chloropropane ND<85 1,12-Trichloroethane ND<85 <br /> Dibromomethane ND<85 Trichloroethene ND<85 <br /> 1 2 Dichlorobenzene ND<85 Tnchlorotluoromethane ND<85 <br /> 1,3-Dichlorobenzene ND<85 1,2 3-Tncliloropiopane ND<85 <br /> 1 4-Diclilorobenzene ND<85 1 2 4-Trimethylbenzene 2200 <br /> Dichlorodifluoromethane ND<85 1 3 5-Trimethylbenzene 600 <br /> IJ-Dichloroethane ND<85 Vim,IAcetate"" ND<85 <br /> 1,2-Dichloroethane ND<85 Vint],Chloride"" ND<85 <br /> 1,1-Dichloroethene ND<85 Xylenes total '°' 21,000 <br /> cis-1,2-Dtchloroethene ND<85 <br /> trans-1 2-Dichloroethene ND<85 <br /> 1,2-Dichloropropane ND<85 <br /> 1,3-Dichloropropane ND<85 <br />' 2 2-Dichloropropane ND<85 Comments <br /> 1,1-Dichloropropene ND<85 Surrogate Reco%crms <br /> cis 1,3-Dichloropropene ND<85 Dibromofluoromethane 100 <br /> trans-1,3-Dichloropropene ND<85 Toluene-d8 97 <br /> Ethylene d:bromide ND<85 4-Bromofluoiobenzene 100 <br /> water and vapor samples are reported:n ug/L,soil and sludge samples in ug/kg,wipes in ughs ipe and all TCLP/SPLP extracts:n ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L Vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chlaroethoxy) ethene (d) 2-hexanone (e) dichloromethane (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (:) liquid sample that contains greater than —5 vol % <br /> sediment (3)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene (m)acetic acid ethenyl ester,(n)chloroethane (a)dimethylbenzenes <br /> DHS Certification No 1644 / Edward Hamilton, Lab Director <br />