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110 Second Avenue South 4D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> htt //u ww mccam bell com E-mail mai cr mecampbell com <br /> Advanced GeoEnvironmental Client Project ID Larry's Auto Date Sampled 10/27/97 <br />' 4005 North Wilson Way <br /> Date Received 10/28/97 <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 10/31-11/03/97 <br /> Client P O Date Analyzed 10/31-11/03/97 <br /> Volatile Organics By CC/MS <br /> EPA method 8260 <br />' Lab ID 82323 <br /> Client ID VW-3 <br /> Matrix W <br /> Com ound Concentration* Com ound Concentration* <br />' Acetone N ND<2600 trans-I 3-Dichloro ro ene ND<1250 <br /> Benzene 38,000 Eth)leve dibronude" ND<1250 <br /> Bromobenzene ND<1250 £thylbenzene 3300 <br /> Bromochloromethane ND<1250 Hexachlorobutadiene ND<1250 <br />' Bromodichloromethane ND<1250 lodomethane ND<1250 <br /> Bromoform ND<1250 Isa ro ylbenzene ND<1250 <br /> Bromomethane ND<1250 -Iso rop)Ito]uene ND<1250 <br /> n-Butyl benzene ND<1250 Methyl butyl ketone'`' ND<1250 <br />' sec-Butyl benzene ND<1250 Meths lene Chloride" ND<1250 <br /> tert-Butyl benzene ND<1250 Meth%I eth)I ketone'' ND<1250 <br /> Carbon Disulfide ND<1250 Methyl isobutNI ketone'"' ND<1250 <br /> Carbon Tetrachloride ND<1250 Methyl Cert-Buhl Ether(MTBE) --- <br /> Chlorobenzene ND<1250 Napthalene ND<1250 <br /> Chloroethane ND<1250 it Prop)] benzene ND<1250 <br /> 2-Chloroethyl Vinv)Ethee'` ND<1250 St\rene"' ND<1250 <br /> Chloroform ND<1250 1 1 12 Tetrachloroethane ND<1250 <br />' Chloromethane ND<1250 1 1 2 2-Tetrachloroethane ND<12A <br /> 2-Chforotoluene ND<1250 Tetrachlomethene ND<1250 <br /> 4-Clilorotoluene ND<1250 Toluene""' 24,000 <br /> Dibromochloromethane ND<1250 1 2 3-Trichloroberizene ND<1250 <br />' 1 2-Dibromo-3-chloro ro ane ND<1250 1 2 4-Trichlorohenzene ND<1250 <br /> Dibromomethane ND<1250 I I I-Trichloroethane ND<1250 <br /> 1 2-Dichlorobenzene ND<1250 I 12-Trichloroethane ND<1250 <br /> I3-Dichlorobenzene ND<1250 Trichloroethene ND<1250 <br />' 14-Dichlorobenzene ND<1250 Tnchlorotluoromethane ND<1250 <br /> Dichlorodifluoromethane ND<1250 1 2 3-Tnchloroprop-im. ND<1250 <br /> 1,1-Dichloroethane ND<1250 1 2 4-Trimeft]benzcsit. 2200 <br /> 12-Dichloroethane 2000 1 3 5-Tnnieth ]benzene ND<1250 <br /> t 1,1-Dichloroethene ND<1250 Vinyl Acetate"" ND<1250 <br /> cis-1 2-Dichloroethene ND<1250 Vin?I Chloride'°' ND<1250 <br /> trans-I 2-Dichloroethene ND<1250 Xvlenes total " 16,000 <br />' 1 2-Dichloro ro ane ND<1250 Comments <br /> 1,3-Dichloro ro ane ND<I250 Surrogate Recoteries(%) <br /> 2,2-Dichloropro ane ND<1250 Dibromolluoromethane 96 <br /> I,I-Dichloro ro ene ND<1250 Toluene-d8 100 <br />' <br /> cis-1,3-Dichloro ropene ND<1250 4-Bromolluorobenzene 98 <br /> water and vapor samples are reported in ug/L,soil and sludge samples to ug/kg «apes in ugf„tpe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L vapor samples 0"ug/L solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this ana])sts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl 2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content (k) ether}Ibcnzene (1) meth)[benzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethane o dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> I <br />