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I110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//wwwmc2Mpbellcom E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID Larrys Auto Date Sampled 06/08/01 <br /> 837 Shaw Road Date Received 06/13/01 <br />' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 06/15-06/19/01 <br /> Client P O Date Analyzed 06/15-06/19/01 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 69658 <br />' Client ID MWl/060801 <br /> Matrix W <br /> Compound Concentration* Pq—ngLumi Compound Concentration* Repowng Lund <br />' W S W S <br /> Acetone(b) ND<75 50 25 trans-1,3-Dichloropmpene ND<5 0 10 50 <br /> Benzene 170 1 0 50 Ethylene dibromide ND<5 0 10 50 <br /> Brornobenzene ND<5 0 10 50 Ethylbenzene 28 10 50 <br />' Bromochioromethane NIX5 0 10 50 Hexachlorobutadiene ND<5 0 50 25 <br /> Bromodichloromethane ND<5 0 10 50 lodomethane ND<5 0 10 so <br /> Bromoform ND<5 0 10 50 Isopropylbenzene ND<5 0 10 50 <br /> Bromomethane ND<5 0 10 5 0 p-lsopropyl toluene ND<5 0 10 50 <br />' n-Butyl benzene ND<5 0 10 50 Methyl butyl ketone ND<5 0 10 50 <br /> sec-Butyl benzene ND<5 0 10 50 Methylene Chlonde` ND<10 10 50 <br /> tert-Butyl benzene ND<5 0 1 0 50 Methyl ethyl ketone ND<5 0 20 10 <br /> Carbon Disulfide ND<5 0 10 50 Methyl isobutyl ketones NIX5 0 10 50 <br /> Carbon Tetrachlonde NIX5 0 10 50 Metnyl tert-Butyl Ether(MTBE) -- 10 50 <br /> Chlombenzene NIX5 0 10 5 0 Naphthalene ND<5 0 50 50 <br /> Chloroethane ND<5 0 10 50 n-Propyl benzene 78 10 5 0 <br /> 2-Chloroethyl Vinyl Ether" ND<5 0 10 50 Styrene ND<5 0 10 50 <br />' Chloroform ND<5 0 10 50 1,1,1,2-Tetrachloroethane ND<5 0 10 50 <br /> Chloromethane ND<5 0 10 50 1,1,2,2-Tetrachloroethane ND<5 0 10 50 <br /> 2-Chlorotoluene ND<5 0 1 0 50 Tetrachloroethene ND<5 0 10 50 <br /> 4-Chlorotoluene ND<5 0 10 50 Toluene 5 8 10 50 <br />' Dibromochloromethane ND<5 0 1 0 50 1,2,3-Tnchlorobenzene ND<5 0 50 25 <br /> 1,2-Dibrorno-3-chloropropane NIM 0 20 10 1,2,4-Tnchlorobenzene ND<5 0 50 25 <br /> Dibromomethane ND<5 0 10 50 1,1,1-Tnchloroethane ND<5 0 10 5 0 <br />' 1,2-Dichlorobenzene NIX5 0 10 50 1,1,2-Tnchloroethane ND<5 0 10 5 0 <br /> 1,3-Dichlorobenzene ND<5 0 10 50 Trichloroethene NIX5 0 10 5 0 <br /> 1,4-Dichlorobenzene ND<5 0 1 0 50 Trichlorofluoromethane ND<5 0 10 5 0 <br /> Dichlorodifluoromethane ND<5 0 10 50 J1!!! <br /> nchloropropane ND<5 0 10 5 0 <br /> 1,1-Dichloroethane ND<5 0 10 50 1Tnmethylbenzene 13 10 5 0 <br /> 1,2-Dichloroethane ND<5 0 10 50 1Tnmethylbenzene ND<5 0 10 5 0 <br /> 1,1-Dichloroethene ND<5 0 10 50 VAcetate m ND<5 0 50 25 <br /> cis-1,2-Dichloroethene ND<5 0 10 5 0 Vinyl Chlonde " ND<5 0 10 50 <br />' trans-l,2-Dichloroethenc ND<5 0 1 0 50 Xylenes,total 17 10 5 0 <br /> 42-Dichloropropane ND<5 0 10 50 Comments <br /> 1,3-Dichloropropane ND<5 0 lo 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<5 0 10 5 0 Dibromoflucromethane 104 <br />' 1,1-Dichloropropene ND<50 10 50 Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND<5 0 10 50 4-Bromofluorobenzene 98 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting lirrnt,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water iTrirmscible sheen is present, (1)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, ) methylbenzene, (m) acetic acid ethenyl ester, (n) <br />' chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton.,Lab Director <br />