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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//www mccampbell com E-mail mam@mecampbell com <br />' Advanced GeoEnvironmental Client Project ID Larrys Auto Date Sampled 06/08/01 <br /> 837 Shaw Road Date Received 06/13/01 <br />' Stockton, CA 95215 'Client Contact Calvrt Lee Date Extracted 06/15-06/19/01 <br /> Client P O Date Analyzed 06/15-06/19/01 <br />' Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 69660 <br />' Client ID MW3/060801 <br /> Matrix W <br /> * Repanmg Limn Reporung Limit <br /> Compound Concentration W S Compound Concentration W S <br />' Acetone N11<2 5 50 25 trans-1,3-Dichloropropene ND<2 5 10 50 <br /> Benzene 55 1 0 50 Ethylene dibromide ND<2 5 10 50 <br /> Bromobenzene ND<2 5 10 50 Ethylbenzene 10 10 50 <br />' Bromochloromethane ND<2 5 10 50 Hexachlorobutadiene ND<2 5 50 25 <br /> Bromodichloromethane ND<2 5 10 50 Iodomethane ND<2 5 1 10 1 50 <br /> Bromoform ND<2 5 1 0 50 lsopropylbenzene 22 10 1 50 <br /> Bromomethane ND<2 5 1 0 1 50 1 p-Isopropyl toluene 64 10 1 50 <br />' n-Butyl benzene 62 10 1 50 Methyl butyl ketone ND<2 5 10 50 <br /> sec-Butyl benzene ND<2 5 10 1 50 Methylene Chloride" ND<2 5 10 50 <br /> tent-Butyl benzene ND<2 5 1 0 50 Methyl ethyl ketone NIX2 5 20 10 <br /> Carbon Disulfide ND<2 5 10 50 Methyl isobutyl ketone ND<2 5 10 50 <br /> M Carbon Tetrachloride ND<2 5 1 0 50 Methyl tert-Butyi Ether(MTBE) -- 10 50 <br /> Chlorobenzene ND<2 5 to 50 Naphthalene ND<2 5 50 50 <br /> Chloroethane ND<2 5 10 50 n-Propyl benzene 15 10 50 <br /> 2-Chloroethyl Vinyl Ether` ND<2 5 10 50 Styrene ItJ ND<2 5 10 50 <br />' Chloroform ND<2 5 to 50 1,1,1,2-Tetrachloroethane NrX2 5 10 50 <br /> Chloromethane ND<2 5 1 0 50 1,1,2,2-Tetrachloroethane ND<2 5 10 50 <br /> 2-Chlorotoluene ND<2 5 10 50 Tetrachloroethene ND<2 5 10 50 <br /> 4-Chicrotoluene ND<2 5 1 0 50 Tolucne 41 10 50 <br />' Dibromochloromethane ND<2 5 1 0 so 1,2,3-Tnchlorobenzene ND<2 5 50 25 <br /> 12-Dibromo-3-chloropropane ND<2 5 20 10 1,2,4-Tnchlorobenzene ND<2 5 50 25 <br /> Dibromomethane ND<2 5 1 0 50 1,1,1-Trichloroethane ND<2 5 10 50 <br /> 1,2-Dichlorobenzene ND<25 10 50 1,1,2-Tnchloroethane ND<25 10 50 <br />' 1,3-Dichlorobenzene ND<2 5 10 5 0 Trichloroethene ND<2 5 10 50 <br /> 1,4-Dichlorobenzene ND<2 5 10 50 Trichlorofluoromethane ND<2 5 10 50 <br /> Dichlorodifluoromethane ND<2 5 1 0 50 1,2,3-Trichloropropane ND<2 5 10 so <br /> ),I-Dichlorocthane ND<2 5 16 50 1,2,4-Tnmethylbenzene ND<2 5 10 50 <br />' 1,2-Dichloroethane ND<2 5 10 50 1,3,5-Tnmethylbenzene 7 7 10 50 <br /> 1,1-Dichloroethene ND<2 5 10 50 Vinyl Acetate m ND<2 5 50 25 <br /> cis-1,2-Dichloroethene ND<2 5 10 50 Vinyl Chloride ' ND<2 5 10 50 <br /> trans-E,2-Dichloroethene ND<2 5 1 0 50 Xylenes,total 53 10 50 <br />' <br /> 42-Dichlotopropane ND<2 5 1 0 50 Comments <br /> 1,3-Dtchloropropane ND<2 5 10 so Surrogate Recoveries(%) <br /> 22-Ihehloropropane ND<2 5 1 0 50 Dtbromofluoromethane 111 <br /> 1,1-Dichloropropene ND<2 5 1 0 50 Toluene-d8 105 <br />' cis-1,3-Dichloropropene ND<2 5 1 0 50 4-Bromofluorobaimne 108 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting hrtut,N/A means analyte not applicable to this' analysis(b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) etherte, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, ) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloraethene,(o)dimethylbenzenes <br />' DHS Certification No 1644 Edward Harnilton, Lab Director <br /> 1 <br />