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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//www mccampbell com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Project ID Larry's Auto Date Sampled 02/16/00 <br /> 4005 North Wilson Way Date Received 02/22/00 <br />' Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 02123-02/29/00 <br /> Client P O Date Analyzed 02123-02/29/00 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 31575 <br /> Client ID MW 7 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> I <br /> Acetone Ob) ND<5 0 trans-1,3-Dichloropropene NO <br /> Benzene 5 3 Ethylene dibromide NO <br /> Bromobenzene NO Ethylbenzene 31 <br /> Bromochloromethane NO Hexachlorobutadiene ND <br />' Bromodtchloromethane NO lodomethane NO <br /> Bromoform NO Isopropylbenzene 64 <br /> Bromamethane NO p-Isopropyl toluene NO <br /> n-Butyl benzene 1 0 Methyl butyl ketone" ND <br /> sec-Butyl benzene 2 7 Methylene Chloride"' ND<5 0 <br /> cert-Butyl benzene 1 6 Methyl ethyl ketone" NO <br /> Carbon Disulfide NO Methyl isobutyl ketone'g ND <br /> Carbon Tetrachloride NO Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane NO n Propyl benzene 13 <br /> 2-Chloroethyl Vm�l Ether"I NO Stvrene" NO <br /> I Chloroform ND 1,1,1,2-Tetrachloroethane NO <br /> Chloromethane NO 1 12,2-Tetrachloroethane NO <br /> 2-Chlorotoluene NO Tetra chloroethene NO <br /> 4-Chlorotoluene ND Toluene'"" 2 7 <br /> Dibromochloromethane NO 1 2,3 Tnchlorobenzene NO <br /> 1,2-Dibromo-3-chloropropane ND 12,4-Tnchlorobenzene NO <br /> Dibromomethane NO 1 1 1 Trichloroethane ND <br /> 1 2-Dichlorobenzene NO 1 1 2 Trichloroethane ND <br /> 13-Dichlorobenzene NO Trichloroethene ND <br /> 1,4-D7ehlOrobenzene NO TnchloroflUOTOmethane NO <br /> Dichlorodifluoromethane ND 1 2 3-Tnchloropropane ND <br /> 1,1-Dichloroethane NO 124-Tnmethyl benzene 35 <br /> I 1 2 Dichloroethane 1 4 1 3 5-Tnmethyl benzene ND <br /> I 1 Dichloroethene ND Vinyl Acetate"' 13 <br /> cis-1,2 Dichloroethene ND \'inyl Chloride` NO <br /> trans-1 2-Dichloroethene ND a,,lenes,total 6 2 <br />' 1 2-Dtchloropropane ND Comments <br /> 1 3-Dichloropropane NO Surrogate Rcco%teies('%) <br /> 2 2-Dtchloropropane NO Dibromofluaromethane 106 <br /> I 1-Dchloropropene ND Toluene-d8 98 <br /> cis 1,3-Dichloropropene NO 4 Bromofluorobenzene 87 <br /> xsater and%apor samples are reported in ug/L soil and sludge samples in uglkg «ipes in ug/%%lpe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated %%ater samples 1 uglL N apor samples 0 5 ug/L,solid and sludge samples 5 uglkg,\s ipes 0 2ug/wipe <br /> ND means not detected above the reporting limit N/A means analvte not applicable to this anal)sis <br /> (h) 2-propanone or dimethyl ketone (c) {2-chloroethox,, ethcne (d) 2 hexanone (e) dichloromethane, (i) 2-bul3none (g) 4-methyl-2 <br /> pentanone or isopiopylacetone (h) hghter than Hater immiscible sheen is present (i) liquid simple that contains greater than —5 vol % <br /> sediment (1) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Ceitificalion No 1644 v d\vaid Hamilton, Lab Director <br /> I <br />