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110 2nd Avenue South,#D7, Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 http//www mccampbell corn E-mail main@mccampbell com <br /> Advanced GeoEnvironrnental Client Project ID Larry's Auto Date Sampled 02/16/00 <br /> 4005 North Wilson Way Date Received 02/22/00 <br />' Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 02123-02/29/00 <br /> Chent P O Date Analyzed 02123-02/29100 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 31578 <br /> Client ID V W 4 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone'i ND<1000 trans-l,3-Dichloropropene ND<1000 <br /> Benzene 23,000 Ethylene dibromide ND<1000 <br /> Bromobenzene ND<1000 Ethvibenzene 4300 <br /> Bromochloromethane ND<1000 Heaachlorobutadiene ND<1000 <br /> I Bramodlchioromelhane ND<1000 lodomethane N13<1000 <br /> Bromoform ND<1000 Isopropyl benzene ND<1000 <br /> Bromomethane ND<1000 p-lsopropyl toluene N13<1000 <br /> n-Butyl benzene ND<1000 Methyl butyl ketoneND<1000 <br /> I sec-Butyl benzene ND<1000 Methylene Chlonde" ND<4000 <br /> tent-Butyl benzene ND<1000 Methyl ethyl ketone" ND<1000 <br /> Carbon Disulfide ND<1000 Methyl isobutyl ketone ND<1000 <br /> Carbon Tetrachloride ND<1000 Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<1000 Naphthalene ND<1000 <br /> Chloroethane ND<1000 n-Propyl benzene ND<3000 <br /> 2-Chloroethyl Vinyl Ether" ND<1000 St)rene` ND<1000 <br /> Chloroform ND<1000 1,1,1,2-Tetrachloroethane ND<1000 <br />' Chloromethane ND<1000 1,1,2,2-Tetrachloroethane ND<1000 <br /> 2-Chlorotoluene ND<1000 Tetrachloroethane 1300 <br /> 4-Chlorotoluene ND<1000 Toluene'"" 32 000 <br />' Dibromocbloromethane ND<1000 1,2 3-Trichlorobenzene ND<1000 <br /> 12-Dibromo-3-chloropropane ND<1000 1,24-Trichlorobenzene ND<1000 <br /> Dibromomethane ND<1000 1,1,1 Trichloroethane ND<1000 <br /> 1,2-Dichlorobenzene ND<1000 1,1,2-Trichloroethane ND<1000 <br />' 13-Dicblorobenzene ND<1000 Trich3oroethene ND<1000 <br /> 14-Dichlorobenzene ND<1000 Trichlorofluoromethane ND<1000 <br /> Dichlorodifluoromethane ND<1000 1 2 3-Trichloropropane ND<1000 <br /> 1,1-1Jichloroethane ND<1000 1 2 4-Trimethylbenzene 3900 <br />' 1,2 Dichloroethane ND<1000 1,3,E Trimelhylbenzene ND<1000 <br /> 1 1-Dichloroethene ND<1000 Vim]Acetate"" ND<1000 <br /> cis 1 2 Dichloroethene ND<1000 Vint]Chloride`) ND<1000 <br /> trans-1,2-Dichloroethene ND<1000 V lenes,total 24,000 <br />' 1 2 Dichloropropane ND<1000 Comments <br /> 1,3 Dichloropropane ND<1000 Surrogate Reco%vries(%} <br /> 2 2-Dichloropropane ND<1000 DibromoflUOTOmethane 108 <br /> 1,1-Dichloropropene ND<1000 Toluene-d8 109 <br />' cis-1,3-Dichlaropropene N13<1000 4-Bronofluorobenzene 102 <br /> eater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ugAk ipe and dll TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated eater samples] ug/L vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg wipes 0 Zug/n ipe <br /> I ND means not detected abo%a the reporting limit NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hewanone (c) dichloromethane, (f) 2 butanone (g)4-methyl-2 <br /> penianone or isoprapvlacetone, (h) lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol % <br /> sediment 0) sample diluted due to high organic content (k) ethemlbenzene (1) nX1hylben2e11e (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethvlbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />