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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> i <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//www mccampbell co m E-mail main@mceampbell com <br /> Advanced GeoEnvirorunental Client Project ID Larry's Auto <br /> Date Sampled 02/16/00 <br /> I4005 North Wilson Way Date Received 02/22/00 <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 02/23-02/29/00 <br />' Client P 0 Date Analyzed 02/23-02129/00 <br /> Volatile Organics By GC/MS <br />' EPA method 8260 <br /> Lab ID 31580 <br /> Client ID VW 5C <br /> Matrix W <br />' Compound Concentration* Compound Concentration* <br /> Acetone 1bj ND<1100 trans-l,3-DichIoropropene ND<650 <br /> Benzene 6600 Ethylene dibromide ND<650 <br /> Bromobenzene ND<650 Elhylbenzene 2700 <br />' Bromochloromethane ND<650 Hexachlorobutadiene ND<650 <br /> Bromodichloromethane ND<650 lodomethane ND<650 <br /> Bromoform ND<650 1 sopropylbenzen e ND<650 <br /> Bromomethane ND<650 p-€soprop)1 toluene ND<650 <br /> n-Butyl benzene ND<650 Methyl butyl ketone` ' ND<650 <br /> sec-Butyl benzene ND<650 Methylene Chloride"' ND<1400 <br /> tert-Butyl benzene ND<650 Methyl ethyl ketone' ND<650 <br /> Carbon Disulfide N13<650 Methyl isobutyl ketone'x' ND<650 <br /> Carbon Tetrachloride ND<650 Methyl tert Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<650 Naphthalene ND<650 <br /> Chloroethane ND<650 n Propyl benzene ND<650 <br />' 2-Chloroe1hyl Vinyl Ether` ND<650 Styrene' ND<650 <br /> Chloroform ND<650 1,1,1,2-Tetrachloroethane ND<650 <br /> Chloromethane N D<650 1,1,2,2-Tetrachloroethane ND<650 <br /> 2-Chlorotoluene ND<650 Tetrachloroethene ND<650 <br />' 4-Chlorotoluene ND<650 Toluene"" 14 000 <br /> Dibromochloromethane ND<650 1,2 3 Tnchloroberizene ND<650 <br /> 1 2-Dibromo-3-chloiopropane ND<650 12,4-Trichlorobenzene ND<650 <br /> Dibromomethane ND<650 1,1 1-Trichloroelhane ND<650 <br />' 1,2-Dichlorobenzene ND<650 1,1 2-Trichloroethane ND<650 <br /> 13-Dichlorobenzene ND<650 Trichloroethene ND<650 <br /> 14-Dichlorobenzene ND<650 TrichIoroiluoromethan e ND<650 <br /> Dichlorodifluoromethane ND<650 1,2,3-Tnchloropropane ND<650 <br /> 1 1-Dichloroethane ND<650 1,2,4-Trimethylbenzene 2400 <br /> 1,2-Dichloroethane ND<650 1,3,5-Trimethylben7ene 830 <br /> 1 1-Dichloroethene ND<650 Vinyl Acetate"` ND<650 <br /> cis-1,2-Dichloroethene ND<650 Vinyl Chloride") ND<650 <br /> I trans-1,2-Dichloroethene ND<650 Xylenes,total 'P 13,000 <br /> 12-Dichloropropane ND<650 Comments <br /> I 3-Dichloropropane ND<650 Surrogate RCCUNlries('%) <br /> 2 2-Dichloropropane ND<650 Dibromofluoromethane 93 <br /> 1,1 Dtchloropropene ND<650 Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND<650 4 Bromofluorobenzene 127 <br /> %Saler and vapor samples are reported in ug/L soli and sludge samples in ug/kg,wipes in ughtipe and all TCLP/SPLP e\tracis in ug/L <br /> Reporting limits unless othem iso slated %%aier samples 1 ug/L,vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg Wipes 0 2ugh%rpe <br /> ND means not detected above the reporting limn NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethox)) ethene, (d) 2-hexanone (c)dichloromethane, (1) 2-butanone (g) 4-meth)]-2- <br /> pentanone or isopropylacetone, (h)lighter than N%aier immiscible sheen is present (i)liquid sample that contains greater than —5 %of % <br /> Sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (]) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)(:methylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />