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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' hap I/www,mccampbell corp. E-mail main@mccampbell coin <br /> Advanced GeoEnvironmental Client Project ID Larry's Auto Date Sampled 03/23/99 <br /> 4005 North Wilson Way Date Received 03/25/99 <br />' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 03/30/99 <br /> Client P O Date Analyzed 03/30/99 <br />' Volatile Organics By GC/MS <br /> EPA method$260 <br /> Lab ID 05830 <br />' Client ID MW2/3-23-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration" <br /> Acetone mi ND<7 trans-1,3-Dichloropropene ND<2 5 <br />' Benzene 89 Ethylene dibromide ND<2 5 <br /> Bromobenzene ND<2 5 Ethylbenzene 14 <br /> Bromochloromethane ND<2 5 Hexachlorobutadiene ND<2 5 <br />' Bromodichloromethane ND<2 5 lodomethane ND<2 5 <br /> Bromoform ND<2 5 Isopropylbenzene ND<2 5 <br /> Bromomethane ND<2 5 p-Isopropyl toluene ND<2 5 <br /> n-Butyl benzene ND<2 5 Methyl bury]ketone` ND<2 5 <br />' sec-Butyl benzene ND<2 5 Methylene Chloride` ND<7 <br /> tent-Butyl benzene ND<2 5 Methyl ethyl ketone i' ND<2 5 <br /> Carbon Disulfide 22 Methyl isobutyl ketone'g ND<2 5 <br /> Carbon Tetrachloride ND<2 5 Methyl tert Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<2 5 Naphthalene 78 <br /> Chloroethane ND<2 5 n-Propyl benzene ND<2 5 <br /> 2-Chloroethyl Vinyl Ether"I ND<2 5 Styrene"I ND<2 5 <br /> Chloroform 57 1,1,1,2-Tetrachloroethane ND<2 5 <br />' Chloromethane ND<2 5 1,1,2,2-Tetrachloroethane ND<2 5 <br /> 2-Chlorotoluene ND<2 5 Tetrachloroethene ND<5 <br /> 4-Chlorotoluene ND<2 5 Toluene m 61 <br /> Dibromochloromethane ND<2 5 1,2,3 Tnchlorobenzene ND<2 5 <br />' 1,2-Dibromo-3-chloropropane ND<25 1,2,4-Trichlorobenzene ND<25 <br /> Dibromomethane ND<2 5 1,1,1-Trichloroethane ND<2 5 <br /> 1,2-Dichlorobenzene ND<2 5 1,1,2-Trichloroethane ND<2 5 <br /> 1,3-Dichlorobenzene ND<25 Trichloroethene ND<25 <br />' 1,4-Dichlorobenzene ND<2 5 Trichlorofluoromethane ND<2 5 <br /> Die hlorodtfluoromethane ND<2 5 1,2,3-Tnchl0r0propane ND<2 5 <br /> 1,1-Dichlaroethane ND<2 5 1,2,4-Tnmethylbenzene I1 <br /> 1,2-Dichloroethane 14 1,3,5-Trimethylbenzene 27 <br />' 10-Dichloroethene ND<2 5 Vinyl Acetate`" ND--2 5 <br /> cis-1,2-Dichloroethene ND<2 5 Vinyl Chloride ° ND<2 5 <br /> trans-1,2-Dichloroethene ND<2 5 Xylenes,total r 53 <br /> 1,2-Dichloropropane ND<2 5 Comments l <br />' 1,3-Dichloropropane ND<2 5 Surrogate Recovcnes(%) <br /> 2,2-Dichloropropane ND<2 5 Dibromofluoromethane 96 <br /> 1,1-Dichloropropene ND<2 5 Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND<2 5 4-Bromofluorobenzene 90 <br />' �waterand vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all f CLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/mpe <br /> I ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chlorcethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropy]acetorie, (h) lighter than water immiscible sheen is present, (t)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1b44Edward Hamilton, Lab Director <br />