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i110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hUp//www,mccamp igll coin E-mail main@mccampbell com <br /> Date Sampled 03/23/99 <br /> Advanced GeoEnvtronmental Client Project ID Larry's Auto <br /> Date Received 03/25/99 <br /> 4005 North Wilson Way <br />' Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 03/30/99 <br /> Client P O Date Analyzed 03/30/99 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 05833 <br />' Client 1D MW7/3-23-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ) ND<7 trans-1,3-Dichloropropene ND <br /> Benzene 41 Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene 15 <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichioromethane ND lodomethane ND <br />' Bromoform ND Isopropylbenzene 12 <br /> Bromometbane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone ND <br />' sec-Butyl benzene ND Methylene Chloride"' ND<4 <br /> tert-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide 96 Methyl isobutyl ketone i ND <br /> Carbon Tetrachloride ND Methyl ten-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene 3 6 <br /> 2-Chloroethyl Vinyl Ether(c) ND Styrene IL, ND <br /> Chloroform 3 5 1,1,1,2-Tetrachloroethane ND <br />' Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetnachloroethene ND<2 <br /> 4-Chlorotoluene ND Toluene(-) 20 <br /> Dibromochloromethane ND 1,2,3-Tnchlorobenzene ND <br />' 1,2-Dibromo-3-chloropropane ND 1,2,4-Tnchlorobenzene ND <br /> Dibromomethane ND 1,1,1-Tnchloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Tnehloroethane ND <br /> 1,3-Dichlorobenzene ND Tnchloroethene ND <br />' 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Tnchloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Tnmethylbenzene 4 6 <br /> 1,2-Dichloroethane ND 1,3,5-Tnmethylbenzene ND <br />' 1,1-1)ichloroethene ND Vinyl Acetate ND <br /> cis-1,2-Dichloroethene ND Vinyl Chlonde ° ND <br /> trans-1,2-Dichloroethene ND Xylenes,total 2 3 <br /> 1,2-Drchloropropane ND Comments <br />' 1,3-Dichloropropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 95 <br /> 1,1-Dtchloropropene ND Toluene-d8 114 <br /> cis-1,3-Dtchloropropene ND 4-Bromofluorobenzene 102 <br />' water and vapor samples are reported in ug1L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples I ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2�hloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (1)liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Harrulton,Lab Director <br />