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a Sequoia 680 Chesapeake Drive Redwood City,CA 94063 (415) 364-9600 FAX(415)364-9233 <br /> 404 N.Wiget line Walnut Creek,CA 94598 (510) 988-9600 FAX(510)988-9673 <br /> 819 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921-9600 FAX(916)921-0100 <br /> Analytical <br /> r,K,f.;r... ::G:rrG,w.};;e xaa -�r:evr.•:r - :::b:%:+. <br /> j 30-A Lindbergh Ave. Matrix: Liquid <br /> } Livermore, CA 94550 r <br /> f.. <br /> Attention: Ailsa Le May QC Sample Group: 6110372-382 Reported: Nov 19, 1996;;$ <br /> 'a..•q!...y...v.v.,..., v::.n• nr.-: :..•,,..:.<::.;;}:•.:.}+:. ;.u,::.+e::.,.;...;.•::.>.v.Gv�::. ..ti Q":5%-,. <br /> cn:,..:»::.wan::.x!•mT.S.YC.s.,.:�<..•n..v:S0-:..r..:r:.....:.:S:n,..Jr.n..t4.:rvn.:L.vw x,.:n.:»..:.:r w.: ...,:.-. }�,..::.�._.:..::::.,v:::n.W . '::Yn :n n....,.:r.,n...:::::i`.,'r,'.�:: <br /> QUALITY CONTROL DATA REPORT <br /> Analyte: Benzene Toluene Ethyl Xylenes Diesel <br /> Benzene <br /> QC Batch#: GG 111596 GC 111596 GC111596 GC111596 SP111296 <br /> 802002A 802002A 802002A 802W2A 8015EXA <br /> Analy. Method: EPA 8020 EPA 8020 EPA 8020 EPA 8020 EPA 8015 <br /> Prep. Method: EPA 5030 EPA 5030 EPA 5030 EPA 5030 EPA 3510 <br /> Analyst: C.Westwater C.Westwater C.Westwater C.Westwater D.Sharma <br /> MS/MSD#: 6110372 6110372 6110372 6110372 BLK111296 <br /> Sample Conc.: N.D. 0.65 ug/L N.D. 1.4 ug/L N.D. <br /> Prepared Date: 11/15/96 11/15/96 11/15/96 11/15/96 11/12/96 <br /> Analyzed Date: 11/15/96 11/15/96 11/15/96 11/15/96 11/13/96 <br /> Instrument I.D.#: HP-2 HP-2 HP-2 HP-2 HP-3A <br /> Conc. Spiked: 20ug/L 20ug/L 20ug/L 60ug/L 300ug/L <br /> Result: 17 19 22 64 210 <br /> MS%Recovery: 85 92 110 104 70 <br /> Dup. Result: 18 22 24 71 190 <br /> MSD %Recov.: 90 107 120 116 63 <br /> RPD: 5.7 15 8.7 11 10 <br /> RPD Limit: 0.25 0-25 0-25 0.25 0-50 <br /> :.......:r::.....:.....r.:,.:.:....„G:a:::..G.....:..a...:xor:.:.::..:..:......:....rr.,:r....:+s,::,.:.u..:.:....:.:.:........4.r...:....n........:.,.:..,r.......r.,•:.r-:.:.+.--,:......,...,r::....,-.......:.......:..r....x....v....,:.:.,. <br /> LCS#: 2LCS111596 2LCS111596 2LCS111596 2LCS111596 LCS111296 <br /> Prepared Date: 11/15/96 11/15/96 11/15/96 11/15/96 11/12/96 <br /> Analyzed Date: 11/15/96 11/15/96 11/15/96 11/15/96 11/13/96 <br /> Instrument I.D.#: HP-2 HP-2 HP-2 HP-2 HP-3A <br /> Conc.Spiked: 20ug/L 20ug/L 20ug/L 60ug/L 300ug/L <br /> LCS Result: 21 21 22 66 230 <br /> LCS %Recov.: 105 105 110 110 77 <br /> LCS 70-130 70-130 70-130 70-130 60-140 <br /> Control Limits <br /> Please Note: <br /> The LCS Is a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> SEQUOIA A LYTICAL,#1271 preparation,and analytical methods employed for the samples. The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure. If <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recoveryis to be used to validate the batch. <br /> 4ject <br /> F **MS=Matrix Spike,MSD=MS Duplicate,RPD=Relative% Difference <br /> anager <br /> 6110372.ALT 45> <br />