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• <br /> Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 <br /> Job Number: C27163 <br /> Account: KFCAI Kleinfelder, Inc.-Irvine <br /> Project: Costco -Tracy, CA <br /> Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch <br /> C27163-IMS L24085.D 1 04/12/13 XB n/a n/a VL763 <br /> C27163-1MSD L24086.D 1 04/12/13 XB n/a n/a VL763 <br /> C27163-1 L24074.D 1 04/12/13 XB n/a n/a VL763 <br /> rn <br /> A <br /> The QC reported here applies to the following samples: Method: SW846 8260B <br /> C27163-1, C27163-2, C27163-3 <br /> C27163-1 Spike MS MS MSD MSD Limits <br /> CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD <br /> 71-43-2 Benzene ND 39.8 33.1 83 31.4 81 5 81-119/20 <br /> 100-41-4 Ethylbenzene ND 39.8 33.6 84 31.5 81 6 80-119/21 <br /> 1634-04-4 Methyl Tert Butyl Ether ND 39.8 39.4 99 37.6 97 5 79-127/19 <br /> 108-88-3 Toluene ND 39.8 33.9 85 31.8 82 6 80-117/21 <br /> 1330-20-7 Xylene (total) NO 120 96.4 81 90.8 78* a 6 81-122/22 <br /> CAS No. Surrogate Recoveries MS MSD C27163-1 Limits <br /> 1868-53-7 Dibromotluoromethane 118% 116% 115% 70-130% <br /> 2037-26-5 Toluene-D8 105% 106% 105% 70-130% <br /> 460-00-4 4-Bromolluorobenzene 107% 107% 100% 70-130% <br /> (a) Outside control limits due to matrix interference. <br /> * = Outside of Control Limits. <br /> 17 of 17 <br /> G ACCUTEST. <br /> 027163 .....1 "1. <br />