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Lancaster <br /> Laboratories Ana 1 ysis Report <br /> 2425 New Holland Pike PQ Box 12425 Lancaster,PA 17605-2425•717-656-2300 Fax 717-658.2681•www lencasterlabs Com <br /> Page 2 of 5 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 850557 <br /> Deported 05/16/03 at 05 09 FM <br /> Laboratory Compliance Quality Control <br /> Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result Pah Unita 9sRE 96REC Limits RPD RPD Max <br /> Xylene (Total) N D 0 5 ug/l 10 84-120 <br /> Sample Matrix Quality Control <br /> I <br /> MS MSD MS/MSD RPD BRG DUP DUP Dup} <br /> RPD <br /> Anal aia Name %RHC %REC Limits RPD MAX Conc Canc RPD Max <br /> I <br /> Batch number 031250020A Sample number($) 4037611-4037614 <br /> Methanol (by Direct In3ection) 104 113 78-116 8 20 <br /> Batch number 03125112601A Sample number(s) 4037615 <br /> TRPH 416 1 77 86 39-132 10 14 1 5 9 5 145* (1) 34 <br /> Batch number 03126A07C Sample number(s) 4037606-4037609 <br /> TPH-GRO - Waters 116 70-130 <br /> Batch number 03127A07B Sample number(s) 4037610-4037615 <br /> TPH-GRO - Waters 115 115 70-130 0 30 <br /> Batch number N031272AS Sample number(s) 4037611-4037615 . <br /> Ethanol 99 112 34-163 13 30 <br /> Methyl Tertiary Butyl Ether 105 106 69-134 0 30 <br /> di-Isopropyl ether 103 102 75-130 1 30 <br /> Ethyl t-butyl ether 100 99 73-123 2 30 <br /> t-Amyl methyl ether 98 99 77-117 2 30 <br /> t-Butyl alcohol 114 118 39-155 3 30 <br /> Benzene (2) (2) 83-128 1 30 <br /> 1,2-Dichloroethane 130 127 73-136 2 30 <br /> Toluene 111 109 83-127 1 30 <br /> 1,2-Dibromoethane 107 106 78-120 1 30 <br /> Ethylbenzene 150* 127 82-134 8 30 <br /> Xylene (Total) 129 116 82-130 6 30 <br /> I <br /> Hatch number N031281AB Sample number(s) 4037610 <br /> Methyl Tertiary Butyl Ether SOB 108 69-134 0 30 <br /> Benzene lie 119 83-128 1 30 <br /> Toluene 111 112 83-127 1 30 <br /> Ethylbenzene 107 108 82-134 1 30 <br /> Xylene (Total) 112 114 82-130 1 30 <br /> Batch number P031331AA Sample number(s) 4037607 <br /> Methyl Tertiary Butyl Ether 100 99 69-134 0 30 <br /> Benzene 108 107 83-128 1 30 <br /> Toluene 102 106 83-127 3 30 <br /> Ethylbenzene 103 104 82-134 0 30 <br /> Xylene (Total) 104 105 82-130 1 30 <br /> Batch number P031332AA Sample number(B) 4037608 <br /> Methyl Tertiary Butyl Ether 97 101 69-134 4 30 <br /> Benzene 105 113 83-128 5 30 <br /> Toluene 103 109 83-127 6 30 <br /> Ethylbenzene 104 111 82-134 6 30 <br /> Xylene (Total) 103 109 82-130 6 30 <br /> I <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br />