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Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364 9600 FAX (415) 364 9233 <br /> 1900 Bates Avenue,Suite L Concord CA 94520 (510) 686 9600 FAX (510) 686 9689 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento CA 95834 (916) 921 9600 FAX (916) 921 0100 <br /> OP08 Services Client Project ID Unocal #6981, 4707 Pacific Ave, Stockton <br /> 2401 Stanwell Dr, Ste 400 Matrix Liquid <br /> Concord, CA 94520 <br /> Attention Avo Avedesslan OC Sample Group 4071480-89 Reported Aug 10, 1994 <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE Benzene Toluene Ethyl Xylenes <br /> Benzene <br /> Method EPA 8020 EPA 8020 EPA 8020 EPA 8020 <br /> Analyst J Fontecha J Fontecha J Fontecha J Fontecha <br /> MS/MSD <br /> Batch# 4071482 4071482 4071482 4071482 <br /> Date Prepared 8/4/94 8/4/94 8/4/94 8/4/94 <br /> Date Analyzed 8/4/94 8/4/94 8/4/94 8/4/94 <br /> Instrument I D # HP-4 HP-4 HP-4 HP-4 <br /> Conc Spiked 20 frg/L 20pg/L 20pg/L 60jtg/L <br /> Matrix Spike <br /> % Recovery 95 100 100 102 <br /> Matrix Spike <br /> Duplicate% <br /> Recovery 95 95 95 98 <br /> Relative% <br /> Difference 00 51 51 4 0 <br /> LCS Batch# 2LCS080494 2LCS080494 2LCS080494 2LCS080494 <br /> Date Prepared 8/4/94 8/4/94 8/4/94 8/4/94 <br /> Date Analyzed 8/4/94 8/4/94 8/4/94 8/4/94 <br /> Instrument I D # HP-4 HP-4 HP-4 HP-4 <br /> LCS % <br /> Recovery 86 95 97 100 <br /> ° Recovery <br /> Control Limits 71-133 72-128 72-130 71-120 <br /> Please Note <br /> The LCS is a control sample of known,interferent free matrix that is analyzed using the same reagents, <br /> SEQUOIA ANALYTICAL, #1271 preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> ignature on File the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> Alan B Kemp interference,the LCS recovery is to be used to validate the batch <br /> Project Manager <br /> 4071480 MPD <4> <br />