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1 <br /> Sequoia 680 Chesapeake Drive Redwood City,CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9600 FAX(510) 988 9673 <br /> Analytical 819 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX(916) 921 0100 <br /> 16D8 Services Client Project ID Unocal #6981, 4707 Pacific Ave Stockton <br /> 2401 Stanwell Dr, Ste 300 Matrix Liquid <br /> Concord, CA 94520 <br /> Attention Jarrel Crider QC Sample Group 7011160-171 Reported Feb 4, 1997 <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE Benzene Toluene Ethyl Xylenes <br /> Benzene <br /> Method EPA 8020 EPA 8020 EPA 8020 EPA 8020 <br /> Analyst K Nill K Nil] K Nill K Nill <br /> MS/MSD <br /> Batch# 7011350 7011350 7011350 7011350 <br /> Date Prepared 1/29/97 1/29/97 1/29/97 1/29/97 <br /> Date Analyzed 1/29/97 1/29/97 1/29/97 1/29/97 <br /> Instrument I D # HP-5 HP 5 HP-5 HP-5 <br /> Conc Spiked 20Mg/L 20pg/L 20ug/L 60lig/L <br /> Matrix Spike <br /> % Recovery 90 85 90 85 <br /> Matrix Spike <br /> Duplicate % <br /> Recovery 85 80 85 80 <br /> Relative % <br /> Difference 5 7 61 57 61 <br /> LCS Batch# 5LCS012997 5LCS012997 5LC8012997 5LCS012997 <br /> Date Prepared 1/29/97 1/29/97 1/29/97 1/29/97 <br /> Date Analyzed 1/29/97 1/29/97 1/29/97 1/29/97 <br /> Instrument I D # HP-5 HP-5 HP-5 HP 5 <br /> LCS % <br /> Recovery 95 85 95 87 <br /> Recovery <br /> Control Limits 60-140 60-140 60-140 60-140 <br /> Please Note <br /> The LCS is a control sample of known,interferent free matrix that is analyzed using the same reagents, <br /> SEQUOIA ANALYTICAL, #1271 preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> eture on File the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> Alan B Kemp interference,the LCS recovery is to be used to validate the batch <br /> Project Manager <br /> 7011160 MPD <7> <br />