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DatE, EDB EDC TAME TBA RIPE ETBE Ethanol Methanol Ethanol Sampled 8260B 8260B 8260B 8260B 8015B 8015B 8260B (Ng/1) (µ811) Gµ811) (nd) (41) (Vgll) (mg/1) (mg/1) (n/1) MW-I1 continued 06/26/00 __ ND<2 00 ND<100 ND<2 00 ND<2 00 09/22/00 ND<2 0 ND<2 0 ND<2 0 ND<50 ND<2 0 ND<2 0 ND<500 ND<]00 -_ 12/26/00 -- -- ND<2 00 ND<100 ND<2 00 ND<2 00 ND<l 000 03/07/01 ND<2 00 ND<2 00 ND<2 00 ND<100 ND<2 00 ND<2 00 ND<l 000 06/26/01 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<l 000 09/12/01 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<t 000 12/12/01 ND<10 ND<10 ND<10 ND<20 ND<10 ND<10 ND<500 -- -- 03/20/02 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<500 -- 06/06/02 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<500 -- -- 09/30/02 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<500 -- -- 12/30/02 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<500 - - 03/29/03 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<500 -- - 06/25/03 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<500 - -- 09/24/03 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 -- ND<500 03/09/04 ND<2 0 -- ND<2 0 ND<100 ND<2 0 ND<2 0 -- -- ND<500 MW-14 08/21/99 -- -- ND<2 0 ND<100 ND<2 0 ND<2 0 ND<500 - -- 10/25/99 ND<2 0 11 ND<2 0 ND<100 ND<2 0 ND<2 0 -- -- -- 01/27/00 ND<2 0 88 ND<2 0 ND<100 ND<2 0 ND<2 0 - - - 06/26/00 ND<4 00 188 ND<4 00 ND<200 ND<4 00 ND<4 00 09/22/00 ND<2 0 10 ND<2 0 ND<50 ND<2 0 ND<2 0 ND<500 ND<l 00 _ 12/26/00 ND<3 34 6 84 ND<3 34 ND<167 ND<3 34 ND<3 34 ND<1 670 03/07/01 ND<2 50 4 14 ND<2 50 ND<125 ND<2 50 ND<2 50 ND<l 250 06/26/01 ND<2 0 3 6 ND<2 0 ND<100 ND<2 0 ND<2 0 ND 09/12/01 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<l 000 -- 12/12/01 ND<10 ND<10 ND<10 ND<20 ND<10 ND<10 ND<500 - -- 03/20/02 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<500 -- -- 06/06/02 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<500 -- - 12/30/02 ND<2 0 ND<2 0 ND<2 0 ND<100 ND<2 0 ND<2 0 ND<500 - - 6981 Page 9 of 15