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Report Number 48134 QC Report Matrix Spike/ Matrix Spike Duplicate Date 2/4/2006 Project Name SINGH'S UNOCAL Project Number 3254 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 48134-06 <0 50 400 400 387 377 ug/L EPA 8260B 1131106 968 944 2 53 70-130 25 Toluene 48134-06 <0 50 400 400 371 364 ug/L EPA 82608 1131106 927 909 1 95 70-130 25 Tert-Butanol 48134-06 <5 0 200 200 180 185 ug/L EPA 82606 1131106 898 92 7 322 70-130 25 Methyl-t-Butyl Ether48134-06 <0 50 400 400 38 3 399 ug/L EPA 8260B 1/31106 957 996 407 70-130 25 Benzene 48134-04 <0 50 400 400 406 400 ug/L EPA 8260B 1/31106 102 100 1 36 70-130 25 Toluene 48134-04 <0 50 400 400 41 0 41 1 ug/L EPA 82606 1/31106 102 103 0 210 70-130 25 Tert-Butanol 48134-04 <5 0 200 200 207 206 ug/L EPA 8260B 1131106 104 103 0 430 70-130 25 Methyl-t-Butyl Ether48134-04 3 9 400 400 467 470 ug/L EPA 8260B 1131/06 107 108 0 668 70-130 25 Benzene 48170-04 <0 50 400 400 418 402 ug/L EPA 82606 1131106 104 101 373 70-130 25 Toluene 48170-04 <0 50 400 400 389 375 ug/L EPA 8260B 1131/06 97 3 937 378 70-130 25 Tert-Butanol 48170-04 <5 0 200 200 213 208 ug/L EPA 8260E 1/31106 107 104 2 33 70-130 25 Methyl-t-Butyl Ether48170-04 <0 50 400 400 388 389 ug/L EPA 8260B 1131106 969 973 0 385 70-130 25 Benzene 48134-01 <0 50 400 400 405 394 ug/L EPA 8260B 1/30106 101 98 5 2 82 70-130 25 Toluene 48134-01 <0 50 400 400 396 385 ug/L EPA 82606 1130/06 990 964 269 70-130 25 Tert-Butanol 48134-01 <5 0 200 200 208 208 ug/L EPA 8260B 1130/06 104 104 0 108 70-130 25 Methyl-t-Butyl Ether48134-01 22 400 400 36 7 363 ug/L EPA 8260B 1/30106 861 853 0 979 70-130 25 i KIFF ANALYTICAL, LLC Approved By Joe iff 2795 2nd St, Suite 300 Davis, CA 95616 530-2974800