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K y <br /> 110 2nd Avenue South,#137,Pacheco, CA 94553-5560 <br /> 1 kCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> • htt /htuw mceanibell coni L-matt main@mccatnpbell coni <br /> Aqua Science Engineers, Inc Client Project ID #3254,Singh's Unocal Date Sampled 1 1101-1 1/02/01 <br /> 208 W El Pintado Road Date Received 11102101 <br /> Danville, CA 94526 Client Contact Robert KitaF Date Extracted 11/05-11106101 <br /> Client P O Date Analvzed 11/05-11106101 <br /> Gasoline Rarge (C6-C12)Volatile hydrocarbons as Gasoline*,with Methyl tert-Butyl Ether* &BTEX*� <br /> LPA methods 5030 modified 8015 and 8030 or 602 California RWQCB(SF Bay Region)method GCP1D(5030) <br /> Lab ID Client ID Matrix TPH(g)4 MTBE Benzene Toluene Ethyl- Xylenes %Recovery <br /> benzene Surrogate <br /> 82590 574/EN11/7 W ND --- ND ND ND ND 105 <br /> 82591 5743301/ W ND 095 1 l ND 2 1 104 <br /> 330 <br /> 82592 574/ENV1/ ND 10 091 ND 1 8 106 <br /> 660 <br /> 82593 574/ENVl/ ND l 1 0 81 ND 1 7 105 <br /> 995k <br /> I <br /> Rep otnirng Limit unless 50 ug/L 5 0 0 0 5 0 5 0 5 <br /> other%�iSL statLd ND <br /> means not detected abo%c <br /> the iLpotung hizut S 1 0 mg/kg 0 OS 0 00� 0 005 0 005 0 005 <br /> " eater and Vapor samples ate reporlLd m 1-1_e11 wipe samples in ughsipe soil and sludge samples in mg/kg and all TCI_P and SDLP LSU tLiS <br /> in ug/L <br /> clutterLd chromatogram samplL�e-ik coeknLs with sunogati,pear, <br /> -1 he coll(+ H> " dLscriptions of N, I PH cliromatowram xL cur,oi) in ndturL and N1LCanipbLll Ail-11%IlLal is not rLsponsible for thus <br /> niterprLtaoon a) unmoditiLd or nezkly moditied�gasoline is signilicant b) hens ier gasohnL iangL compounds are signihcant(agLd <br /> gasoline`') c) lighter gasoline range compounds (the most mobile haction) arc significant d) gdsolmL range compounds liming brotd <br /> • chromatographic peaks are sognificant biologically alta-rt d gasoline" (.)T PH pattern that dols not appLar to be deri\ed from gasolmL <br /> one to a ton isolated peaks present g)strongly aged gasoline or diesel range compounds ate significant h) lighter than nater inirril ciblL <br /> sheen is present r)hquA sample that contains grLater than—5 sol %sediment i)no recognizable pattem <br /> DHS CLitification No 1644 Edward Hamilton, Lab Directoi <br />