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110 2nd Avenue South ##D7 Pacheco CA 94553-5560 <br /> F4 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> hap ilwww inccampbell com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental,Inc Client Project ID Granthrie Gas&Food Date Sampled 09/19/02 <br /> 837 Shaw Road Date Received 09/24/02 <br />' Stockton,CA 95215 Client Contact Brian Millman Date Extracted 09/26/02-09/27/02 <br /> Client P O Date Analyzed 09/26/02-09/27/02 <br />' Oxygenated Volatile Organics by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SWE26013 Work Order 0209368 <br />' Lab ID 0209368-001B f 0209368-002B j 0209368-003B 0209368-004B <br /> Client lD MW1/091902 MW2/091902 I MW3/091902 MW4/091902 Reporting Limit for <br /> i <br />' Matrix W W f W W DP=t <br /> DF 1 i 1 - 1 1 S W <br /> Compound Concentration -T ug/kg µg/L <br /> Dnsopropyl ether(DIPS) NO ND ND ND NA 05 <br />' Ethyl tert-butyl ether(ETRE) ND ND ND ND NA 05 <br />' Methyl-t-butyl ether(MTBE) 12 ND 063 057 NA 05 <br /> tent-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> l <br /> t-Butyl alcohol(TBA) ND ND ND ND NA 50 <br /> ie <br /> Surrogate Recoveries(%} <br />' %SS 984 993 995 977 <br /> Comments <br />' *water and vapor samples and all TCLP&SPLP extracts are reported in ug/L,soil/sludge/solid samples in ug/kg, wipe samples in ug/wipe, <br /> productloil/non-aqueous liquid samples in mg/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,l)sample diluted due to high <br /> organic content <br /> 1 ' <br /> I <br /> 1 <br /> I <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />