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110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br />' MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 h92//www mccamybell com E-mail main@mccampbelI com <br /> 1 Advanced GeoEnvironmental Client Project ID Grantiine Gas&Food Date Sampled 09/17/01 <br /> 837 Shaw Road Date Received 09/19/01 <br /> 1 Stockton,CA 95215 Client Contact Brian Millman Date Extracted 09/24-09126101 <br />' Client P O Date Analyzed 09/24-09126/01 <br /> Oxygenated Volatile Organics By GC/MS- <br /> EPA method 8260 modified <br />' Lab ID 78809 78810 78811 78812 <br /> MW51 MW6/ MW7/ MW8/ Reporting Limit <br /> Client ID 091701 091701 091701 091701 <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(D1PE) ND ND ND ND 5 0 10 <br />' Ethyl tert-Butyl Ether(ETRE) ND ND ND ND 50 10 <br /> lie Methyl-tert Butyl Ether(MTBE) ND ND 17 45 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 1 0 <br />' tert-Butanol ND ND ND ND 25 50 <br />' Surrogate Recoveries(%) <br />' Dibromofluoromethane 104 103 115 114 <br /> Comments <br />' *water samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br />' (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,{1)sample diluted due to <br /> high organic content <br />' DHS Certification No 1644 Edward Hamilton,Lab Director <br />