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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCANDBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> harp//yA Mccampbell conn E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Protect ID Grantlme Gas &Food Date Sampled 09/12/00 <br /> 4005 North Wilson Way Date Received 09/13/00 <br /> Stockton,CA 95205 Client Contact Bnan Millman Date Extracted 09/15-09/20/00 <br /> Client P O Date Analyzed 09/15-09120/00 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />` Lab ID 47439 47440 47441 47442 <br /> IMWI/ MW2/ MW3/ MW4/ Reporting Limit <br /> Client TD 09-12-00 09-12-00 09-12-00 09-12-00 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND<2 0 ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND<2 0 ND ND ND 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) 67 ND ND 55 50 10 <br /> tent-Amyl Methyl Ether(TAME) ND<2 0 ND aND <br /> ND 50 10 <br /> Itent-Butanol ND<10 ND ND 25 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 122 123 122 123 <br /> Comments <br />' *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/vnpe and all TCLP I STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br />' (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than-5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> r <br />' DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />