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110 2nd Avenue South,#FD7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hap//www,mccampbell co m E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project 1D Grantline Gas&Food Date Sampled 12/21/99 <br /> 4005 North Wilson Way Date Received 12122199 <br /> Stockton, CA 95205 Client Contact Bill Little Date Extracted 12/25-12/27/99 <br /> Client P O Date Analyzed 12125-12127/99 <br /> Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br /> Lab ID 28043 28044 28045 28046 <br /> Reporting Limit <br /> Client ID MW1 MW2 MW3 MW4 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND NO NO ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBF) NO NO NO ND 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) 13 NO NO 11 50 1 0 <br /> tent-Amyl Methyl Ether(TAME) NO ND NO ND 50 1 0 <br /> tert-Butanol ND ND NO ND 25 so <br /> ISurrogate RecoN cries <br /> Dibromofluoromcthan e 106 104 110 118 <br /> IComments <br /> *later samples are reported in ug/L,soil and sludge samples in ug/kg,vopes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (i)hqukd sample that contains greater than —5 %ol %sediment,0)sample diluted due to <br /> high organic content <br /> iDHS Certification No 1644 Edward Hamilton, Lab Director <br /> i <br /> I <br />