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' r 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' hM2://www.mccauMbel l.co E-mail mam@mccampbell com <br />' Advanced GeoEnviromnental Client Protect ID Grantline Gas&Food Date Sampled 03/25/99 <br /> 4005 North Wilson Way Date Received 03/31/99 <br />' Stockton,CA 95205 Client Contact Bill Little Date Extracted 04103-04105/99 <br /> CIient P O Date Analyzed 04/03-04/05/99 <br />' Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 08248 08249 08250 08251 <br />' <br /> Client ID MWl/3-25- MW2/3-25- MW3/3-25- MW4/3-25- Reporting Limit <br /> 99 99 99 99 <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(D1PE) ND<5 ND ND ND<3 so 10 <br />' Ethyl tert-Butyl Ether(ETBE) ND<5 ND ND ND<3 50 10 <br /> Methyl-tert Butyl Ether(MTBE) 190 ND ND 110 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND<5 ND ND ND<3 50 10 <br />' tert-Butanol ND<25 ND ND ND<15 25 50 <br /> tSurrogate Recoveries{%) <br /> Dibromolluoromethane 96 95 95 92 <br /> 1 <br /> Comments h <br />' *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L. <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br />' (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic content <br />' DHS Certification No 1644 Edward Hamilton,Lab Director <br />