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10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http Ilwww mccampbell com E-mail matn@mccampbell cam <br />' Advanced GeoEnvironmental Client ProJect ID #0111,Grantline Gas& Date Sampled 06/18/98 <br /> Food Date Received 06/20/98 <br />' 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 06/25/98 <br />' Client P O Date Analyzed 06/25/98 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br />' Lab ID 90886 <br /> Client ID MW6/6-18-98 <br /> Matrix W <br />' Compound Concentration* Compound Concentration* <br /> Acetone ' ND<5 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br />' Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone` ND <br /> Bromomethane ND Methylene Chloride" ND <br />' n-Butyl benzene ND Methyl ethyl ketoneND <br /> sec-Butyl benzene ND Methyl isobutyl ketone'x ND <br /> tert-Butyl benzene ND Methyl teri-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Naphthalene ND<15 <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene ' ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br />' 2-Chloroethyl Vinyl Ether") ND 1,1 2 2-Tetrachloroethane ND <br /> Chloroform ND Tctrachloroethene ND <br /> Chloromethane ND Toluene"' ND <br /> 2-Chlorotoluene ND 1 2 3-Tnchlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Trichlorobenzene ND <br /> Dibromochloromethane ND 111-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1 12-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br />' 1,2-Dichlorobenzene ND Trichlorotluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2 3-Trichloropropane ND <br /> 1,4-Dichlorobenzene ND 124-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Trimethylbenzene ND <br />' <br /> 1,1-Dichloroethane ND Vinyl Acetate""I ND <br /> 1,2-Dich]oroethane ND Vinyl Chloride"` ND <br /> 1,1-Dichloroethene ND Xylenes,total '° ND <br /> cis-1,2-Dichloroethene ND <br />' trans-1,2-Dichloroethene ND <br /> 1,2-Dic11101"opropane ND <br /> 1,3-Dichlorop170pane ND <br /> 2,2-Dichloropropane ND Comments <br />' 1,1-Dichloropropene ND Surrogate Reco%eries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethanc 115 <br /> trans-1,3-Dichloropropene ND Toluene-d8 108 <br /> Ethylene dibromide ND 4-Bromotluorobenzene 100 <br />' water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes to uglwipe and all TCLP I SPLP extracts m ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 Zug/wipe ND means not detected above the reporting limit NIA means analyte not applicable to this analysts <br />' 1b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene (d) 2-hexanone, (e)dichloromethane, (i) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than--5 vol % <br /> sediment,0)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1}methylbenzene (m)acetic acrd ethenyl ester,(n}chloro ethene,(o)d i methLylbenzcnes <br /> DHS Certification No 1644 // Edward Hamilton, Lab Director <br />