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Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> 111W Analytical 819 Striker Avenue Su.tc 8 Sacramento CA 95834 (916) 921 9600 FAX(916)921 Moo <br /> • <br /> Touchstone Development Client Project ID Chevron 9-4183 <br /> 781 Kingston Matrix Solid <br /> Oakland, CA 94611 <br /> Attention Robert Mallory Work Order# 9604898 06, 07 Reported Apr 23, 1996 <br /> QUALITY CONTROL DATA REPORT <br /> Analyte 1,2,4-Trlchloro 4-Chloro-3 Acenaphthene 4-Nitrophenol <br /> benzene Methylphenol <br /> OC Batch# M80415968270EXA MSO415968270EXA MSO415968270EXA MSO415968270EXA <br /> Analy Method EPA 8270 EPA 8270 EPA 8270 EPA 8270 <br /> Prep Method EPA 3550 EPA 3550 EPA 3550 EPA 3550 <br /> Analyst <br /> MS/MSD# <br /> Sample Conc <br /> Prepared Date <br /> Analyzed Date. <br /> Instrument I D # <br /> Conc. Spiked <br /> Result- <br /> MS % Recovery: <br /> Dup Result: <br /> MSD % Recov.. <br /> RPD: <br /> RPD Limit <br /> LCS # SBG41596 SBO41596 S8041596 SBN1596 <br /> Prepared Date 4/15/96 4/15/96 4/15/96 4/15/96 <br /> Analyzed Date 4/15/96 4/15/96 4/15/96 4/15/96 <br /> Instrument I D #. F4 F4 F4 F4 <br /> Conc Spiked 3300 pg/Kg 3300ug/Kg 3300 ug/Kg 3300pg/Kg <br /> LCS Result 2600 2600 2400 2300 <br /> LCS % Recov 79 79 73 70 <br /> LCS 40-120 40-120 50-140 20-120 <br /> Control Limds <br /> Please Note <br /> The LCS 1s a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> .SE000 A ANALYTICAL preparation,and analytical methods employed for the samples The matrix spike 1s an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> Interference,the LCS recovery is to be used to validate the batch <br /> Kevin Follett **MS=Matrix Spike,MSD=MS Duplicate, RPD=Relative% Difference <br /> Project Manager Page 2 of 3 9604898TTT <3> <br />