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Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 404 N Wiget Lane Walnut Creek CA 94598 (510) 988 9600 FAX (510) 988 9673 <br /> VjV Analytical 819 Striker Avenue,Suite 8 Sacramento CA 95834 (916) 921 9600 FAX(916) 921 0100 <br /> Touchstone Developments Client Project ID Chevron 9-4183 /9-4183 <br /> 781 Kingston Matrix Solid <br /> Oakland, CA 94611 <br /> Attention Robert Mallory Work Order# 9604750 01-06 Reported Apr 15, 1996 <br /> QUALITY CONTROL DATA REPORT <br /> Analyte Beryllium Cadmium Chromium Nickel <br /> QC Batch# ME0411966010MDE ME041196601OMDE ME041196601OMDE ME041196601OMDE <br /> Analy. Method EPA 6010 EPA 6010 EPA 6010 EPA 6010 <br /> Prep Method EPA 3050 EPA 3050 EPA 3050 EPA 3050 <br /> Analyst S O'Donnell S O'Donnell S O'Donnell S ODonnell <br /> MS/MSD # 960467001 960467001 960467001 960467001 <br /> Sample Cone : N D ND 23 18 <br /> Prepared Date 4/11/96 4/11/96 4/11/96 4/11/96 <br /> Analyzed Date 4/11/96 4/11/96 4/11/96 4/11/96 <br /> Instrument I D # MTJA2 MTJA2 MTJA2 MTJA2 <br /> Cone Spiked 100 mg/Kg 100 mg/Kg 100 mg/Kg 100 mg/Kg <br /> Result 78 78 100 96 <br /> MS % Recovery 78 78 77 78 <br /> Dup Result 51 52 67 66 <br /> MSD % Recov 51 52 44 48 <br /> RPD 42 40 40 37 <br /> RPD Limit 0-30 0-30 0-30 0-30 <br /> LCS# BLK041196 BLK041196 BLK041196 BLK041196 <br /> Prepared Date 4/11/96 4/11/96 4/11/96 4/11/96 <br /> Analyzed Date 4/11/96 4/11/96 4/11/96 4/11/96 _ <br /> Instrument I D # MTJA2 MTJA2 MTJA2 MTJA2 <br /> Conic Spiked 100 mg/Kg 100 mg/Kg 100 mg/Kg 100 mg/Kg <br /> LCS Result 100 100 100 100 <br /> LCS % Recov.. 100 100 100 100 <br /> LCS 75-125 75-125 75-125 75-125 <br /> Control Limits <br /> Please Note <br /> The LCS 1s a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br />• <br /> SEGUQJA ANALYTICAL preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch <br /> Kevin Follett <br /> Project Manager **MS=Matrix Spike,MSD=MS Duplicate, RPD=Relative%Difference 9604750 TTT <2> <br />