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COLUMBIA ANALYTICAL SERVICES, INC. <br /> I <br /> Analytical Report <br /> Client: EMCON Associates Service Request: S941406 <br /> Project: TOSCO# l 1191 /0952-089.02 bate Collected 11/8194 <br /> Sample Matrix: Soil Date Received: 11/9/94 <br /> Date Extracted: NA <br /> Halogenated Volatile Organic Compounds I <br /> EPA Methods 5030/80I0 <br /> Units: mg/Kg(ppm) , <br /> As Received Basis i <br /> Sample Name: Method Blank <br /> Lab Code: S9411 10-SB <br /> Date Analyzed:. 11/10/94 <br /> Analyte MRL <br /> Dichlorodifluoromethane(CFC 12) 0.1 ND <br /> Chloromethane 0.1 ND <br /> Vinyl Chloride 0.05 ND <br /> Bromomethane 0.05 ND <br /> Chloroethane 0.05 ND <br /> Trichlorofluoromethane(CFC 11) 0,05 ND <br /> 1,1-Dichloroethene 0.05 ND <br /> Trichlorotrifluoroethane(CFC 113) 0.05 ND <br /> Methylene Chloride 0.05 ND <br /> trans-I,2-Dichlo roethene 0.05 ND <br /> cis-1,2-Dichioroethene 0.05 ND <br /> 1,I-Dichloroethane 0,05 ND <br /> Chloroform 0.05 ND l <br /> 1,1,1-Trichloroethane(TCA) 0.05 ND <br /> f Carbon Tetrachloride 0.05 ND <br /> 1,2-Dichloroethane 0.05 ND <br /> Trichloroethene(TCE) 0,05 ND <br /> 1,2-Dichloropropane 0.05 ND <br /> Bromodichloromethane 0.05 ND <br /> 2-Chloroethyl Vinyl Ether 0.5 ND <br /> trans-1,3-Diehl oropropene 0.05 ND <br /> c is-1,3-D ichloropropene 0.Q5 ND <br /> 1,1,2-Trichloroethane 0.05 ND <br /> Tetrachloroethene(PCE) 0.05 ND <br /> Dibromochloromethane 0.05 ND r <br /> Chlorobenzene 0.05 <br /> ND <br /> B ro moform 0.05 ND <br /> 1,1,2,2-Tetrachloroethane 0.05 ND + <br /> 1,3-Dichlorobenzene 0,1 ND - <br /> 1,4-Dichlorobenzene 0.1 ND <br /> 1,2-D ichIorobenzene 0.1 ND #A <br /> I <br /> Approved By: Date: <br /> 3S44W394 - <br /> Page 7 of l I <br />