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� ! i Report Number 30647 QC Report Matrix Spike/Matrix Spike Duplicate Date 116103 Project Name Beacon Project Number 3641 Stockton Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 30665-02 <0 50 400 400 400 38 3 ug/L EPA 82606 113103 100 958 4 39 70-130 25 Toluene 30665-02 <0 50 400 400 337 323 ug/L EPA 82608 113103 843 808 4 21 70-130 25 Tert-Butanol 30665-02 <5 0 200 200 214 210 ug/L EPA 82606 113103 107 105 1 62 70-130 25 Methyl-t-Bury!Ether 30665-02 <0 50 400 400 424 398 ug/L EPA 8260B 113103 106 995 623 70-130 25 Benzene 30648-03 180 400 400 221 221 ug/L EPA 8260B 112103 105 104 0 334 70-130 25 Toluene 30648-03 38 400 400 720 749 ug/L EPA 82606 112103 ' 83 9 91 0 812 70-130 25 Tert-Butanol 30648-03 2100 200 200 2340 2260 ug/L EPA 8260B 112103 120 788 41 3 70-130 25 Methyl-t-Butyl Ether 30648-03 2600 400 400 2550 2650 ug/L EPA 8260B 112103 000 139 200 70-130 25 Benzene 30647-07 <0 50 400 400 402 401 ug/L EPA 8260E 12/30/02 100 100 0 224 70-130 25 Toluene 30647-07 <0 50 400 400 396 387 ug/L EPA 82606 12/30/02 989 968 212 70-130 25 Tert-Butanol 30647-07 <5 0 200 200 198 202 ug/L EPA 82606 12/30/02 990 101 2 09 70-130 25 Methyl-t-Butyl Ether 30647-07 072 400 400 404 403 ug/L EPA 82606 12/30/02 991 989 0202 70-130 25 Benzene 30654-12 5 3 400 400 446 433 ug/L EPA 8260B 112103 984 950 3 54 70-130 25 Toluene 30654-12 16 400 400 55 9 542 ug/L EPA 8260B 112103 100 965 4 14 70-130 25 Tert-Butanol 30654-12 120 200 200 316 313 uglL EPA 82606 112103 969 952 1 80 70-130 25 Methyl-t-Butyl Ether 30654-12 140 400 400 185 186 ug/L EPA 8260B 112103 •104 106 215 70-130 25 V'fa q Approved By Jbel Kiff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800