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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client AlZCO ProdULK Company <br /> Service Request: S9700986 <br /> Proles-t 21775-206 00vT0A21333 00/548 %TOCKTON Date Collected. 5127/97 <br /> SdmPh, M.itrie Water <br /> Date Received: 5/28/97 <br /> BTEX,MTBE and TPH as Gasoline <br /> Sample Name MW-4(6 1) <br /> Lab Code 59700986-004 Units ug/L(ppb) <br /> Test Notes Basis NA <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CA/LUTT 50 I NA 6/5197 ND <br /> Benzene EPA 5030 8020 05 I NA 6/5/97 ND <br /> Toluene EPA 5030 8020 0 5 1 NA 6/5/97 ND <br /> Ethylbenzene EPA 5030 8020 05 1 NA 6/5/97 ND <br /> Xylenes Total EPA 5030 8020 05 1 NA 6/5/97 ND <br /> Methyl 1er1-Butyl Ether EPA 5030 8020 3 1 NA 6/5/97 ND <br /> is221020597p ISI <br /> Page 6 <br />