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Pace Analyilcal Services,Inc. 900 Gemini Avenue ;acemaocal- Houston, 58 Phone 281 48&1848b[1810 www pacelabs com Fax 281488.4661 Lab Project Number 8529658 Client Project ID Site 11193- relogs 8528842 Lab Sample No 851770826 Project Sample Number 8529658-001 Date Collected 07/29/02 15 10 Client Sample ID MN-3 (ORIa 851763391) CA Matrix water Date Received 08/01/02 09 20 Parameters Results Units Report Limit DF Analyzed. B CAS No ggal Re Lm n-Propylbenzene ND ug/1 500 100 09/16/02 18 44 EAD 103-65-1 1,2,3-Trichlorobenzens ND ug/1 100 100 09/16/02 18 44 SAD 87-61-6 1,2,4-Trichlorobenzens ND ug/1 100 100 09/16/02 18 44 LAD 120-82-1 1,2,3-Trimethylbenzene ND ug/1 100 100 09/16/02 18 44 EAD 526-73-8 1,2,4-Trimethylbenzene ND ug/1 100 100 09/16/02 18 44 EAD 95-63-6 1,3,5-Trlmsthylbenzene ND ug/1 100 100 09/16/02 18 44 EAD 108-67-8 Bromobenzene ND ug/1 500 100 09/16/02 18 44 K= 108-86-1 Hexachloro-1,3-butadiene ND ug/1 200 100 09/16/02 18 44 EAD 87-68-3 Rexachloroethane ND ug/l 200 100 09/16/02 18 44 FAD 67-72-1 2-Methyl-2-propanol ND ug/1 1000 100 09/16/02 18 44 EAD 75-65-0 Ethyl-tart-butyl ether ND ug/1 200 100 09/16/02 18 44 EAD 637-92-3 Diisopropyl ether ND ug/l 200 100 09/16/02 18 44 EAD 108-20-3 tert-Amylmethyl ether ND ug/l 200 100 09/16/02 18 44 EAD 994-05-8 Toluene-d8 (S) 105 % 1 0 09/16/02 18 44 EAD 2037-26-5 4-Bromofluorobenzene (S) 88 % 1 0 09/16/02 18 44 EAD 460-00-4 1,2-Dlchloroethane-d4 (S) 104 % 1 0 09/16/02 18 44 EAD 17060-07-0 • Comments Relogs There was significant headspace in the VOA vial Proceed with analysis, per client request Analysis conducted in excess of EPA recommended holding time Data 09/17/02 Papa 3 of 34 i REPORT OF LABORATORY ANALYSIS This report shaft not be reproduced except in toll without the written consent of Pace Analytics[Services Inc