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Pace Analytical Services,Inc 9100 Gemini Avenue � 7X 77058 acemalyt�cal n � 'r 488 1810 www paeelabs coni Fax 281488 4661 Lab Pr03ect Number. 8529658 Client Project ID Site 11193- relogs 8528842 Lab Sample No 851770828 Project Sample Number 8529658-003 Date Collected. 07/29/02 14.40 Client Sample ID HW-9 (ORIG 8517633991 Matrix Water Date Received 08/01/02 09 20 Parameters _ Results Units Report Limit DF Analyzed By CAS NO, Qual ROOLMt n-Propylbenzene ND ug/l 5 0 1 0 09/17/02 07.42 MAD 103-65-1 1,2,3-Trichlorobenzene ND ug/l 1 0 1 0 09/17/02 07.42 HAD 87-61-6 1,2,4-Trichlorobenzene ND ug/l 1 0 1.4 09/17/02 07 42 MAD 120-82-1 1,2,3-Trimethylbenzens ND ug/I 1 0 1 0 09/17/02 07 42 EAD 526-73-8 1,2,4-Trimethylbenzene ND ug/l 1.0 1 0 09/17/02 07 42 SAD 95-63-6 1,3,5-Trlmethylbenzens ND ug/l 1 0 1 0 09/17/02 07 42 HAD 108-67-8 Bromobenzene ND ug/l 5 0 1 0 09/17/02 07 42 BAD 108-86-1 Hexachloro-1,3-butadiene ND ug/l 2 0 1 0 09/17/02 07 42 EAD 87-68-3 Hexachloroethane ND ug/l 2 0 1 0 09/17/02 07 42 EAD 67-72-1 2-Methyl-2-propanol 3100 ug/l 1000 100 09/17/02 07 42 PAD 75-65-0 Ethyl-tert-butyl ether ND ug/l 2 0 1 0 09/17/02 07 42 MAD 637-92-3 Diisopropyl ether ND ug/l 2 0 1 0 09/17/02 07 42 EAD 108-20-3 tart-Amyluethyl ether 86 ug/l 2 0 1 0 09/17/02 07 42 HAD 994-05-8 Toluene-d8 (S) 102 % 1 0 09/17/02 07 42 PAD 2037-26-5 4-Bromofluorobenzene (S) 105 % 1 0 09/17/02 07 42 MAO 460-00-4 1,2-Dichloroethane-d4 (S) 84 % 1 0 09/17/02 07 42 MAD 17060-07-0 • Comments Relogs There was significant headspace in the VOA vial. Proceed with analysis, per client request Analysis conducted in excess of EPA reccmmended holding tlm8 IN �r s � Date 09/17/02 Page 9 of 34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full without the wntten consent of Pace AnaMul Services Inc