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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report , `' <br /> Client: EMCON Associates Service Request: 5941510 <br /> Project: TOSCO#11193/0952-091.02 Date Collected: 11/22/94 <br /> Sample Matrix: Sail Date Received: 11/22/94 <br /> Date Extracted: 11/30!94 <br /> Date Analyzed: I2/3,4/94 <br /> Hydrocarbon Scan <br /> California DHS LUST Method <br /> Units: mg/Kg(ppm) <br /> As Received Basis <br /> Mineral TPH as <br /> Analyte: Spirits Jet Fuel Kerosene Diesel Hydraulic Oil <br /> Method Reporting Limit: 1 1 1 1 5 <br /> Sample Name Lab Code <br /> 11193-TPHIS-10 5941510-001 ND ND ND I * ND <br /> 11193-TPHIS-15 5941510-002 ND ND ND ND ND. <br /> 11193-7PH2S-10 5941510-003 ND ND ND ND ND <br /> 11193-TPH2S-15 5941510-004 ND ND ND ND ND <br /> 11193-TD-2 5941510-005 840 ** <20 *** <20 *** 7,600**** <100**^ <br /> 11193-TD-3 S941510-006 800 ** <10 *** <10 *** 3,400 **** <50*** <br /> Method Blank 5941130-SB ND ND ND ND ND <br /> * This sample contains a lower boiling point hydrocarbon mixture, quantified as diesel. The chromatogram does <br /> not match the typical diesel fingerprint. -._ <br /> ** This sample contains components eluting in the mineral spirits range,quantified as mineral spirits. The chromatogram <br /> does not snatch the typical mineral spirits fingerprint <br /> *** Raised MRL due to high analyte concentration requiring sample dilution. <br /> **** This sample contains a mixture of diesel and lower boiling point hydrocarbons,quantified as diesel. The chromatogram <br /> does not match the typical diesel fingerprint. <br /> Approved By: Date: (� �1 � <br /> SAMRa9. - <br />