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Entech Anal tical Labs Inc. <br /> 3334 Victor Court , Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201 <br /> ATC Associates Inc.-Pleasanton Project ID: 75.62503.3206 <br /> 6602 Owens Drive,Suite 100 Project Name: Quik Stop 4132 <br /> Pleasanton,CA 94588 <br /> Attn: Scott Perkins Project Location: Stockton <br /> GlobalID: T0607700418 <br /> Certificate of Analysis - Data Report Samples Received: 07/26/2006 <br /> Sample Collected by: Client <br /> Lab#: 50595-003 Sample ID: 4202 (Drum 1-2) Matrix: Solid Sample Date: 7/25/2006 <br /> EPA 8021E <br /> Parameler Result Qual D/P-F Detection Limit Units Prep Dale Prep Batch Analysis Date QC Batch <br /> Benzene ND l0 0.10 mglKg 7/2612006 SGCA060726A 7/26/2006 SGCA060726A <br /> Toluene ND 10 0.10 mg/Kg 7/26/2006 SGCA060726A 7/26/2006 SGCA060726A <br /> Ethyl Benzene ND 10 0.10 mg/Kg 7/26/2006 SGCA060726A 7/26!2006 SGCA060726A <br /> Xylenes,Total ND 10 0.10 mg/Kg 7/26/2006 SGCA060726A 7/26/2006 SGCA060726A <br /> Surrogate Surrogate Recovery Control Limits(%) Analyzed by: mruan <br /> 4-Bromolluorobenzene 106 65 - 135 Reviewed by: dba <br /> ICP Metals on TCLP extracts by EPA 60108 <br /> Parameter Result Qual DIP-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch <br /> Lead ND 1.0 0.25 mg/L 8/4/2006 WMTCLP060804 8/7/2006 WMTCLP060804 <br /> Analyzed by: EQueja <br /> Reviewed by: Hdinh <br /> EPA 8021B <br /> AnLrameter Result Qual DIP-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch <br /> ethyl-t-butyl Ether ND 10 0.50 mg/Kg 7/26/2006 SGCA060726A 7/2612006 SGCA060726A <br /> Surrogate Surrogate Recovery Control Limits(%) Analyzed by: mruan <br /> 4-Bromotluorobenzene 106 65 - 135 Reviewed by: dba <br /> TPH-Volatile:EPA 8015B <br /> Parameter Result Qual D/P-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch <br /> TPH as Gasoline ND 10 5.0 mglKg 7/26/2006 SGCA060726A 7/26/2006 SGCA060726A <br /> Surrogate Surrogate Recovery Control Limits(%) Analyzed by: mruan <br /> 4-Bromoflumabenzene 95.6 65 - 135 Reviewed by: dba <br /> TKI-Extractable:EPA 8015E <br /> Parameter Result Qual DIP-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch <br /> TPH as Diesel ND I.0 2.5 mg/Kg 8/2/2006 SD060802A 8/4/2006 SDO60802A <br /> l7 mg/Kg Hydrocarbon(C18-08). <br /> Surrogate Surrogate Recovery Control Limits(%) Analyzed by: ]Hsiang <br /> o-Terphenyl 73.4 41 137 Reviewed by: dba <br /> Detection Limit=Detection Limit for Reporting. ND=Not Detected at orabove the Detection Limit. <br /> D/P-F=Dilution and/or Prep Factor includes sample volume adjustments. Qua[=Data Qualifier 8182006 2:11:20 PM•Kwwffe <br />