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American Environmental Network <br /> WORK ORDER 9805012 QUALITY CONTROL REPORT PAGE QR-3 <br /> ANALYSIS Volatile GUMS <br /> MATRIX Soil/Bulk <br /> METHOD BLANK SAMPLES <br /> SAMPLE TYPE Blank-Method/Media blank LAB ID BLNK 0512 INSTR RUN GCMS131980512000000/l/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED — BATCH ID MS13SO51398 <br /> UNITS ug/kg ANALYZED 05/12/98 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT M <br /> 1,2 DCA-d4 (surr) 101 100 101 60 140 <br /> Toluene-d8 (surr) 104 100 104 65 135 <br /> p BFB (surr) 105 100 105 65 135 <br /> 1 1 Dichloroethene ND 5 <br /> Benzene NO 5 <br /> Trichloroethene NO 5 <br /> Toluene NO 5 <br /> Chlorobenzene NO 5 <br /> Bromobenzene ND 5 <br /> Bromochloromethane ND 5 <br /> Bromodlchloromethane ND 10 <br /> Bromoform NO 5 <br /> ' Bromomethane NO 10 <br /> n Butylbenzene NO 5 <br /> sec Butylbenzene NO 5 <br /> tert Butylbenzene NO 5 <br /> Carbon Tetrachlor,de ND 5 <br /> Chloroethane ND 10 <br /> Chloroform ND 5 <br /> Chloromethane NO 14 <br /> 2 Chlorotoluene NO 5 <br /> 4 Chlorotoluene ND 5 <br /> Dibromochloromethane ND 5 <br /> 1,2 Dibromo 3 chloropropan ND 5 <br /> 1 2 Dibromoethane NO 5 <br /> Dibromomethane NO 5 <br /> 1,2-Dichlorobenzene ND 5 <br /> 1 3-Dichlorobenzene NO 5 <br /> 1 4 Dichlorobenzene NO 5 <br /> Dichlorodifluoromethane NO 10 <br /> 1 1 Dichloroethane NO 5 <br /> 1,2 Dichloroethane ND 5 <br /> cis 1 2 Dichloroethene ND 5 <br /> trans 1 2 Dichloroethene ND 5 <br /> 1,2 Dichloropropane ND 5 <br /> 1,3 Dichloropropane ND 5 <br /> 2 2 Dichloropropane NO 5 <br /> 1,1 Dichloropropene NO 5 <br /> Ethylbenzene ND 5 <br /> Hexachlorobutadiene ND 5 <br /> Isopropylbenzene ND 5 <br /> ' pISO propyltoluene NO 5 <br /> Methylene Chloride NO 10 <br /> Naphthalene NO 5 <br /> n-Propylbenzene ND 5 <br /> Styrene ND 5 <br /> 1,1 1 2-Tetrachloroethane ND 5 <br /> 1,1,2 2-Tetrachloroethane ND 5 <br /> Tetrachloroethene ND 5 <br /> 1 2 3 Trzchlorobenzene ND 5 <br /> 1,2,4 Trichlorobenzene ND 5 <br /> 1 1 1 Trichloroethane ND 5 <br /> 1 1,2 Trichloroethane ND 5 <br /> Trichlorofluoromethane ND 5 <br /> 1 2 3-Trichloropropane NO 5 <br /> 1,2 4 Trimethylbenzene NO 5 <br /> 1 3,5 Trimethylbenzene ND 5 <br /> Vinyl Chloride ND 10 <br /> Xylenes Total ND 10 <br /> I0 Tr,chlorotrifluoroethane NO 5 <br /> Acetone ND 100 <br /> Acrylonitrile NO 10 <br /> 2 Butanone NO 100 <br /> I <br />