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ANALYTICAL RESULTS <br /> NOTotal Petroleum Hydrocarbons By GC <br /> EI/GTEL Client ID: CES06CES0b <br /> gin Number: W7070539 <br /> rProject ID (number),: 97736-01-01 Method: GC <br /> Project ID (name): EGGIMAN/MODESTO/CA Matrix: Solids <br /> NEI/GTEL Sample Number W7070539-01 W7070539.02 W7070539-03 W7070539-04 <br /> r Client iD ET-S81.15.0 ET-SBI-30.0 ET-SB2.15.0 ET-SB3.20.0 <br /> Date Sampled 07/24/97 07/24/97 07/24/97 07/24/97 <br /> Date Prepared 08/02/97 08/02/97 08/02/97 08/02/97 <br /> Date Analyzed 08/07/97 08/07/97 08/07/97 08/07/97 <br /> r Dilution Factor 10.0 1.00 1.00 1.00 <br /> r <br /> Reporting <br /> Analyte Limit Units Concentration Wet Weight <br /> TPS as: Di esl .......... /. 9 :::' ::.;: 1104.;s. . `.l 10 < 10 <br /> Percent Solids -- % 87.4 70.8 83.8 80.0 <br /> rNotes: <br /> Dilution Factor: <br /> Dilution factor indicates the adjustments made for sample dilution. <br /> r GC. <br /> Extraction by EPA Method 3550 (sonication). ASTM Method D3328(modified) is used for qualitative identification of fuel patterns. The method has been <br /> modified to include quantitation by applying calibration and quality assurance guidelines outlined in "Test Methods for Evaluating Solid Waste, <br /> r Physical/Chemical Methods". SW-846. Third Edition including promulgated Update 1. This method is equivalent to the California LOFT manual DHS method <br /> for diesel fuel. <br /> W7070539-01: <br /> ke <br /> alitative identification of diesel fuel is uncertain because the material present does not match laboratory standards. The material is primarily in range C9 to C16. Surrogate spike recovery is outside of acceptability limits therefore the reported concentration should be considered an estimate, <br /> r <br /> r <br /> r <br /> n <br /> i <br /> 1 <br /> 1 <br /> r <br /> *I/GTEL Wichita, KS <br /> rW7070539 Page: 1 <br /> r <br />