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Report Number 33304 QC Report Matrix Spike/ Matrix Spike Duplicate Date 6/3/2003 Project Name JOES TRUCK PLAZA Project Number 9627-001-4 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 33288-01 <0 50 400 400 424 394 ug/L EPA 8260B 5124103 106 985 724 70-130 25 Toluene 33288-01 <0 50 400 400 420 386 ug/L EPA 8260B 5124103 105 966 834 70-130 25 Tert-Butanol 33288-01 <50 200 200 204 191 ug/L EPA 8260E 5124103 102 954 666 70-130 25 Methyl-t-Butyl Ether 33288-01 23 400 400 646 609 ug/L EPA 8260B 5124103 103 943 913 70-130 25 Benzene 33304-10 <0 50 400 400 417 41 1 ug/L EPA 8260E 5127103 104 103 133 70-130 25 Toluene 33304-10 <0 50 400 400 402 401 ug/L EPA 8260B 5127103 100 100 0 324 70-130 25 Tert-Butanol 33304-10 <5 0 200 200 200 194 ug/L EPA 8260E 5127/03 999 968 313 70-130 25 Methyl-t-Butyl Ether 33304-10 <0 50 400 400 418 409 ug/L EPA 82608 5127/03 105 102 222 70-130 25 Benzene 33359-04 <0 50 400 400 378 392 ug/L EPA 82608 5131/03 946 980 356 70-130 25 Toluene 33359-04 <0 50 400 400 392 408 ug/L EPA 82608 5131/03 981 102 382 70-130 25 Tert-Butanol 33359-04 <5 0 200 200 195 205 ug/L EPA 8260B 5/31103 974 102 502 70-130 25 Methyl-t-Butyl Ether 33359-04 <0 50 400 400 437 462 ug/L EPA 8260B 5/31103 109 116 554 70-130 25 Benzene 33286-02 <0 50 400 400 394 395 ug/L EPA 82608 5124/03 986 988 0 253 70-130 25 Toluene 33286-02 <0 50 400 400 432 429 ug/L EPA 82608 5124103 108 107 0 883 70-130 25 Tert-Butanol 33286-02 <5 0 200 200 209 210 ug/L EPA 8260E 5124103 104 105 0 468 70-130 25 Methyl-t-Butyl Ether 33286-02 <0 50 400 400 384 389 ug/L EPA 8260E 5124/03 961 972 1 19 70-130 25 V, ,J i Approved By Jpel Kiff KIFF ANALYTICAL, LLC f 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800