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Submission: 2004-12-0056 <br /> STL <br /> Gas/BTEX Fuel Oxygenates by 8260B <br /> TRC Alton Geoscience-Irvine <br /> Attn.:Anju Farfan <br /> 21 Technology Drive <br /> Irvine, CA 92718 <br /> Phone: (949) 341-7440 Fax: (949) 753-0111 <br /> Project: 41050001 FA20 Received: 11/30/2004 16:07 <br /> Conoco Phillips#11195 <br /> Site: 16500 S. Interstate 5 <br /> Batch QC Report <br /> Prep(s): 50308 Test(s):.82601FAB <br /> Matrix Spike (MS!MSD ) Water QC Batch#200411.2106-2A.64 <br /> MW-5 >> MS Lab ID: 2004-12-0056-005 <br /> MS: 2004112106-2A.64-050 Extracted: 12/07/2004 Analyzed: 12107/2004 01:50 <br /> Dilution: 1.00 <br /> MSD: 2004112106-2A.64-013 Extracted:12/07/2004 Analyzed: 12107/2004 02:13 <br /> Dilution: 1.00 <br /> Compound Conc. ug 1L Spk.Level Recove % Limits% Flags <br /> M5 MSD Sample .,/L MS I MSD RPD Rec. RPD MS MSD <br /> Methyl ter!-butyl ether 913 115 62.9 25 200.4 208.4 3.9 65-165 20 M4 M4 <br /> Benzene 32.0 32.8 ND 25 128-0 131.2 2.5 69-129 20 M4 <br /> Toluene 31.0 32.4 ND 25 124.0 129.6 4.4 70-130 20 <br /> Surrogate(s) <br /> 1,2-Dichluroelhane-d4 446 524 500 89.2 104.8 73-130 <br /> Toluene-d8 464 490 500 96.8 98.0 81-114 <br /> Severn Trent Laboratories, Inc. 121141200413:37" <br /> STL San Francisco`1220 Quarry Lane,Pleasanton,CA 94566 <br /> Apad or Sevam Trent Plc Tel 925 484 1919 Fax 925 484 1096`www.stl-inc.com'CA DHS ELAP#2496 Page 41 of 50 <br />