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P%1 :..ata File : /var/chem/n . i/n980513 . b/nl33cwl . d Page 1 Report Date : 13 -May-1998 15 : 34 SPL Houston Labs CONTINUING CALIBRATION COMPOUNDS zstrument ID : n . i Injection Date : 13-MAY-1998 14 : 25 Lab File ID : n133cwl .r1 Init . Calibration Dates? : 05/01/98 05/01/98 Analysis Type : WATER Init . Calibration Times : 14 : 14 16 : 04 ' b Sample ID : VSTD050-8250W Method File : /var/chem/n. i/n980513 . b/n8260wL .m �.'1ant Type : ISTD MIN I I MAX 1 COMPOUND I RRF I RF250 1 RRF 1 tD { %D 1 1 1 Dichlorodifluoromethane 1 0.3951 0.30510.0101 22.71 40.01 1 2 Chloromethane 1 1 0711 1.03410.3001 3.41 40.01 1 3 Vinyl Chloride 1 0.5211 0.52310.100{ -0.21 20.01 -- 1 4 Bromomethane 1 0.22S1 0.22910.1001 -2.11 40.01 I 5 Chloroethane 1 0,3071 0.29810.0101 3.01 40.D1 I 6 Trichlorofluoromethane 1 0.4661 0.47710.0101 -2.41 40.01 1 7 Acetone 1 0.0391 0.04910.0101 -23.21 40,01 1 8 1,1-Dichloroethene 1 0.344 1 0.356610.1001 -3.61 20.01 1 9 Methylene Chloride 1 0.4961 0,52910.0101 -6.61 40.01 1 10 Carbon Disulfide 1 1.283( 1.35110.0101 -5.31 40.01 1 11 trans-1,2-Dichloroethene 1 0.4531 0.52210.0101 -15 31 40.01 1 12 1,1-Dichloroethane 1 1.0011 1.21010.3001 -20.81 40.01 1 13 Vinyl Acetate 1 2.2331 2.12610.0101 4.8f 40.01 1 14 2-3utanone 1 1.5561 1.73010-0101 -11.21 40.01 1 15 cis-1,2-Dichloroethene 1 0.5021 0.57510.0101 -14.5} 4D.01 IM 16 1,2-Dichloroethene (total) 1 0.4771 0.54810.0101 -14.91 40.01 1 1 17 2,2-Dichlorooropane I 0.6971 0.72210.0101 -5.11 40.01 1 18 Bromochloromethane 1 0.:931 0.23910.0101 -23.01 40.01 1 19 Chloroform 1 0.9211 1.07110.2001 -16.31 20.01 IS 21 1,2-Dichloroethane-d41 0.0721 0.08010.0101 -11.21 49.01 f 22 1,1,1-Trichloroethane I 0.5091 0.49510.1001 2.91 40.01 23 1,2-Dichloroethane 1 1,047{ 1.24210.1041 -16 61 40.01 J 24 1,1-Dichloropropene 1 0.7631 0.77310,0101 -1.41 40.01 : 1 25 Benzene 1 1.3601 1.402[0.1001 -3.11 40.C1 J 26 Carbon Tetrachloride 1 0.347[ 0.33610.1001 3.11 40.D1 1 26 1,2-Dichloropropane 1 0.4034 0.42310,0101 -4.91 20.01 29 Trichloroethene [ 0-2831 0.29210.1001 -3.21 40,01 -- 1 30 Dihromomethane 1 0-1961 0,20710.0101 -11.41 40.01 1 31 Bromodichloromethane ( 0.4851 0.51610-2001 -6.61 4D.01 1 32 2-Chloroethylvinylether 1 0.222[ 0.21910.010[ 1.51 40.01 33 4-Methyl-2-Pentanone 1 0.445[ 0.46010.0101 -3.41 40.01 1 34 cis-1,3-Dichloropropene 1 0.5451 0.53710.1001 1.41 40.01 35 trans-1,3-Dichloropropene 1 0.4011 0.47810.1001 2.61 40.01 15 36 Toluene-dB 1 1.3091 1.24210.0101 5.11 40.01 1 37 Toluene ,1 0.8991 0,85910.4001 4.51 20.01 1 38 1,1,2-Trichloroethane 1 0.259[ 0.28210.1001 -9.21 40,01 I I 1 1 I I I F s,