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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-29164-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-74289 Preparation: 5030B <br /> MS Lab Sample ID: 720-29177-A-2 MS Analysis Batch: 720-74289 Instrument ID: CHMSV2 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 07081040.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 07/09/2010 0515 Final Weight/Volume: 10 mL <br /> Date Prepared: 07/09/2010 0515 <br /> MSD Lab Sample ID: 720-29177-A-2 MSD Analysis Batch: 720-74289 Instrument ID: CHMSV2 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 07081041.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 07/09/2010 0548 Final Weight/Volume: 10 mL <br /> Date Prepared: 07/09/2010 0548 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 89 92 60-140 3 20 <br /> 1,1-Dichloroethane 93 96 60-140 3 20 <br /> Dichlorodifluoromethane 69 70 38-140 2 20 <br /> Vinyl chloride 85 90 58-140 6 20 <br /> Chloroethane 91 96 51 -140 5 20 <br /> Trichlorofluoromethane 106 106 60-140 0 20 <br /> Methylene Chloride 105 108 40-140 3 20 <br /> trans-1,2-Dichloroethene 91 94 60-140 3 20 <br /> cis-1,2-Dichloroethene 100 101 60-140 0 20 <br /> Chloroform 97 98 60-140 0 20 <br /> 1,1,1-Trichloroethane 111 111 60-140 0 20 <br /> Carbon tetrachloride 121 121 60-140 0 20 <br /> 1,2-Dichloroethane 99 99 60-140 0 20 <br /> Trichloroethene 93 94 60-140 1 20 <br /> 1,2-Dichloropropane 97 99 60-140 2 20 <br /> Dichlorobromomethane 123 123 60-140 0 20 <br /> trans-1,3-Dichloropropene 115 115 60-140 0 20 <br /> cis-1,3-Dichloropropene 114 116 60-140 2 20 <br /> 1,1,2-Trichloroethane 103 103 60-140 0 20 <br /> Tetrachloroethene 88 87 60-140 2 20 <br /> Chlorodibromomethane 125 125 60-140 0 20 <br /> Chlorobenzene 92 94 60-140 2 20 <br /> Bromoform 115 116 56-140 1 20 <br /> 1,1,2,2-Tetrachloroethane 97 100 60-140 3 20 <br /> 1,3-Dichlorobenzene 95 97 60-140 2 20 <br /> 1,4-Dichlorobenzene 94 96 60-140 3 20 <br /> 1,2-Dichlorobenzene 97 99 60-140 2 20 <br /> Chloromethane 80 86 52-140 8 20 <br /> Bromomethane 92 97 23-140 6 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 88 90 60-140 2 20 <br /> TestAmerica San Francisco Page 24 of 27 07/21/2010 <br />