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QC Sample Results C <br /> Client: Environmental Cost Management, Inc. TestAmerica Job ID: 720-36837-1 <br /> Project/Site: Nestle-Ripon <br /> Method: EPA 524.2 - PURGEABLE ORGANIC COMPOUNDS BY GC/MS (EPA 524.2) (Continued) <br /> Lab Sample ID: 11H2455-MS1 Client Sample ID: RC-1 <br /> Matrix:Water Prep Type: Total <br /> Analysis Batch: 11H2455 Prep Batch: 11H2455_P <br /> Sample Sample Spike Matrix Spike Matrix Spike %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D 0/6 Rec Limits <br /> 1,4-Dichlorobenzene ND 10.0 10.1 Ug/1 101 70-130 <br /> 1,1-Dichloroethane ND 10.0 11.5 ug/I 115 70-130 <br /> 1,2-Dichloroethane ND 10.0 10.5 ug/I 105 70-130 <br /> 1,1-Dichloroethene 0.140 10.0 11.4 ug/I 113 70-130 <br /> cis-1,2-Dichloroethene ND 10.0 9.32 ug/I 93 70-130 <br /> trans-1,2-Dichloroethene ND 10.0 12.3 ug/I 123 70-130 <br /> 1,2-Dichloropropane ND 10.0 9.86 ug/I 99 70-130 <br /> cis-1,3-Dichloropropene ND 10.0 8.99 ug/I 90 70-130 <br /> trans-1,3-Dichloropropene ND 10.0 9.14 ug/I 91 70-130 <br /> Methylene chloride ND 10.0 12.1 ug/I 121 70-130 <br /> 1,1,2,2-Tetrachloroethane ND 10.0 11.2 ug/I 112 70-130 <br /> Tetrachloroethene ND 10.0 9.51 ug/I 95 70-130 <br /> 1,1,1-Trichloroethane ND 10.0 9.48 ug/I 95 70-130 <br /> 1,1,2-Trichloroethane ND 10.0 10.0 ug/I 100 70-130 <br /> Trichloroethene ND 10.0 9.91 ug/I 99 70-130 <br /> Trichlorofluoromethane ND 10.0 10.8 ug/I 108 70-130 <br /> Vinyl chloride ND 10.0 11.5 ug/I 115 70-130 <br /> Matrix Spike Matrix Spike <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene 96 70-130 <br /> 1,2-Dichlorobenzene-d4 104 70-130 <br /> Lab Sample ID: 11H2455-MSD1 Client Sample ID: RC-1 <br /> Matrix:Water Prep Type: Total <br /> Analysis Batch: 11H2455 Prep Batch: 11H2455_P <br /> Sample Sample Spike Matrix Spike Dup Matrix Spike Dul %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Bromodichloromethane ND 10.0 10.2 ug/I 102 70-130 0.9 20 <br /> Bromoform ND 10.0 11.8 ug/I 118 70-130 6 20 <br /> Bromomethane ND 10.0 11.0 ug/I 110 70-130 0 20 <br /> Carbon tetrachloride ND 10.0 11.0 ug/I 110 70-130 2 20 <br /> Chlorobenzene ND B 10.0 9.06 ug/I 91 70-130 0.8 20 <br /> Chloroethane ND 10.0 11.4 ug/I 114 70-130 2 20 <br /> Chloroform ND 10.0 11.0 ug/I 110 70-130 0.6 20 <br /> Chloromethane ND L C 10.0 13.0 ug/I 130 70-130 2 20 <br /> Dibromochloromethane ND 10.0 12.0 ug/I 120 70-130 4 20 <br /> 1,2-Dibromoethane(EDB) ND 10.0 9.28 ug/I 93 70-130 5 25 <br /> 1,2-Dichlorobenzene ND 10.0 9.53 ug/I 95 70-130 6 20 <br /> 1,3-Dichlorobenzene ND 10.0 9.40 ug/I 94 70-130 6 20 <br /> 1,4-Dichlorobenzene ND 10.0 9.72 ug/I 97 70-130 4 20 <br /> 1,1-Dichloroethane ND 10.0 11.7 ug/I 117 70-130 2 20 <br /> 1,2-Dichloroethane ND 10.0 11.9 ug/I 119 70-130 13 20 <br /> 1,1-Dichloroethene 0.140 10.0 11.7 ug/I 116 70-130 2 20 <br /> cis-1,2-Dichloroethene ND 10.0 9.36 ug/I 94 70-130 0.4 20 <br /> trans-1,2-Dichloroethene ND 10.0 12.5 ug/I 125 70-130 1 20 <br /> 1,2-Dichloropropane ND 10.0 9.80 ug/I 98 70-130 0.6 20 <br /> cis-1,3-Dichloropropene ND 10.0 8.85 ug/I 88 70-130 2 20 <br /> trans-1,3-Dichloropropene ND 10.0 8.80 ug/I 88 70-130 4 20 <br /> Methylene chloride ND 10.0 12.1 ug/I 121 70-130 0.2 20 <br /> TestAmerica San Francisco <br /> Page 35 of 49 08/23/2011 <br />