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QC Sample Results C <br /> Client: Environmental Cost Management, Inc. TestAmerica Job ID: 720-37346-1 <br /> Project/Site: Nestle-Ripon <br /> Method: EPA 524.2 - PURGEABLE ORGANIC COMPOUNDS BY GC/MS (EPA 524.2) (Continued) <br /> Lab Sample ID: 1111555-MSD1 Client Sample ID:7501 KIERNAN 2008 EFF <br /> Matrix:Water Prep Type:Total <br /> Analysis Batch: 1111555 Prep Batch: 1111555_P <br /> Sample Sample Spike Aatrix Spike Dup Matrix Spike Dul %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D 0/6 Rec Limits RPD Limit <br /> 1,2-Dichlorobenzene ND 10.0 10.8 ug/1 108 70-130 3 20 <br /> 1,3-Dichlorobenzene ND 10.0 10.5 ug/I 105 70-130 2 20 <br /> 1,4-Dichlorobenzene ND 10.0 10.7 ug/I 107 70-130 2 20 <br /> 1,1-Dichloroethane ND 10.0 9.70 ug/I 97 70-130 2 20 <br /> 1,2-Dichloroethane ND 10.0 10.5 ug/I 105 70-130 5 20 <br /> 1,1-Dichloroethene ND 10.0 9.27 ug/I 93 70-130 0.8 20 <br /> cis-1,2-Dichloroethene ND 10.0 9.65 ug/I 96 70-130 2 20 <br /> trans-1,2-Dichloroethene ND 10.0 9.68 ug/I 97 70-130 1 20 <br /> 1,2-Dichloropropane ND 10.0 10.1 ug/I 101 70-130 2 20 <br /> cis-1,3-Dichloropropene ND 10.0 10.6 ug/I 106 70-130 4 20 <br /> trans-1,3-Dichloropropene ND 10.0 10.9 ug/I 109 70-130 5 20 <br /> Methylene chloride ND 10.0 9.64 ug/I 96 70-130 3 20 <br /> 1,1,2,2-Tetrachloroethane ND 10.0 12.1 ug/I 121 70-130 9 20 <br /> Tetrachloroethene ND 10.0 9.34 ug/I 93 70-130 1 20 <br /> 1,1,1-Trichloroethane ND 10.0 9.61 ug/I 96 70-130 1 20 <br /> 1,1,2-Trichloroethane ND 10.0 11.2 ug/I 112 70-130 7 20 <br /> Trichloroethene ND 10.0 9.51 ug/I 95 70-130 1 20 <br /> Trichlorofluoromethane ND 10.0 9.36 ug/I 94 70-130 0.1 20 <br /> Vinyl chloride ND 10.0 9.63 ug/I 96 70-130 0.3 20 <br /> Matrix Spike Dup Matrix Spike Dup <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene 104 70-130 <br /> 1,2-Dichlorobenzene-d4 109 70-130 <br /> Method: 300.0 -Anions, Ion Chromatography <br /> FLab Sample ID: MB 720-98584/14 Client Sample ID: Method Blank <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 98584 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Nitrate as N ND 0.23 mg/L 09/07/11 11:52 1 <br /> rLab Sample ID: LCS 720-98584/15 Client Sample ID: Lab Control Sample <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 98584 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Nitrate as N 2.26 2.24 mg/L 99 90-110 <br /> Lab Sample ID: 720-37346-2 MS Client Sample ID: 7501 KIERNAN 2008 MID <br /> Matrix:Water Prep Type:Total/NA <br /> Analysis Batch: 98584 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> Nitrate as N 2.6 2.26 4.61 mg/L 88 80-120 <br /> TestAmerica San Francisco <br /> Page 28 of 41 09/20/2011 <br />