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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-31232-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-80483 Preparation: 5030B <br /> MS Lab Sample ID: 720-31232-12 Analysis Batch: 720-80483 Instrument ID: HP5 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 102310017.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/23/2010 1835 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/23/2010 1835 <br /> MSD Lab Sample ID: 720-31232-12 Analysis Batch: 720-80483 Instrument ID: HP5 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 102310018.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/23/2010 1908 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/23/2010 1908 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 113 109 60-140 4 20 <br /> 1,1-Dichloroethane 114 109 60-140 5 20 <br /> Dichlorodifluoromethane 77 86 38-140 11 20 <br /> Vinyl chloride 75 92 58-140 20 20 <br /> Chloroethane 81 90 51 -140 10 20 <br /> Trichlorofluoromethane 89 99 60-140 10 20 <br /> Methylene Chloride 110 104 40-140 6 20 <br /> trans-1,2-Dichloroethene 117 112 60-140 4 20 <br /> cis-1,2-Dichloroethene 126 120 60-140 5 20 <br /> Chloroform 116 110 60-140 6 20 <br /> 1,1,1-Trichloroethane 115 110 60-140 5 20 <br /> Carbon tetrachloride 116 111 60-140 4 20 <br /> 1,2-Dichloroethane 119 111 60-140 6 20 <br /> Trichloroethene 119 113 60-140 5 20 <br /> 1,2-Dichloropropane 122 115 60-140 5 20 <br /> Dichlorobromomethane 131 122 60-140 7 20 <br /> trans-1,3-Dichloropropene 127 120 60-140 6 20 <br /> cis-1,3-Dichloropropene 135 127 60-140 6 20 <br /> 1,1,2-Trichloroethane 129 119 60-140 8 20 <br /> Tetrachloroethene 119 113 60-140 6 20 <br /> Chlorodibromomethane 127 118 60-140 7 20 <br /> Chlorobenzene 112 108 60-140 4 20 <br /> Bromoform 119 112 56-140 6 20 <br /> 1,1,2,2-Tetrachloroethane 110 102 60-140 8 20 <br /> 1,3-Dichlorobenzene 115 110 60-140 5 20 <br /> 1,4-Dichlorobenzene 106 101 60-140 5 20 <br /> 1,2-Dichlorobenzene 110 104 60-140 6 20 <br /> Chloromethane 84 94 52-140 11 20 <br /> Bromomethane 78 87 23-140 11 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 109 104 60-140 5 20 <br /> TestAmerica San Francisco Page 51 of 77 <br />