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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-31232-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-80500 Preparation: 5030B <br /> MS Lab Sample ID: 720-31232-13 Analysis Batch: 720-80500 Instrument ID: HP5 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 102410008.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/24/2010 1329 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/24/2010 1329 <br /> MSD Lab Sample ID: 720-31232-13 Analysis Batch: 720-80500 Instrument ID: HP5 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 102410009.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/24/2010 1401 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/24/2010 1401 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 103 103 60-140 0 20 <br /> 1,1-Dichloroethane 106 105 60-140 1 20 <br /> Dichlorodifluoromethane 75 75 38-140 0 20 <br /> Vinyl chloride 76 74 58-140 2 20 <br /> Chloroethane 81 80 51 -140 1 20 <br /> Trichlorofluoromethane 92 91 60-140 2 20 <br /> Methylene Chloride 99 99 40-140 1 20 <br /> trans-1,2-Dichloroethene 108 107 60-140 0 20 <br /> cis-1,2-Dichloroethene 116 116 60-140 1 20 <br /> Chloroform 105 105 60-140 0 20 <br /> 1,1,1-Trichloroethane 106 104 60-140 2 20 <br /> Carbon tetrachloride 107 106 60-140 1 20 <br /> 1,2-Dichloroethane 108 111 60-140 2 20 <br /> Trichloroethene 109 108 60-140 2 20 <br /> 1,2-Dichloropropane 113 113 60-140 0 20 <br /> Dichlorobromomethane 119 121 60-140 1 20 <br /> trans-1,3-Dichloropropene 119 123 60-140 3 20 <br /> cis-1,3-Dichloropropene 127 128 60-140 1 20 <br /> 1,1,2-Trichloroethane 116 120 60-140 4 20 <br /> Tetrachloroethene 109 107 60-140 1 20 <br /> Chlorodibromomethane 117 121 60-140 3 20 <br /> Chlorobenzene 103 102 60-140 1 20 <br /> Bromoform 113 118 56-140 5 20 <br /> 1,1,2,2-Tetrachloroethane 98 104 60-140 6 20 <br /> 1,3-Dichlorobenzene 107 105 60-140 2 20 <br /> 1,4-Dichlorobenzene 98 97 60-140 1 20 <br /> 1,2-Dichlorobenzene 101 102 60-140 1 20 <br /> Chloromethane 84 84 52-140 0 20 <br /> Bromomethane 77 76 23-140 1 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 99 99 60-140 1 20 <br /> TestAmerica San Francisco Page 56 of 77 <br />