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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-31395-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-80856 Preparation: 5030B <br /> MS Lab Sample ID: 720-31364-A-20 MS Analysis Batch: 720-80856 Instrument ID: CHMSV2 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 10291030.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/29/2010 2339 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/29/2010 2339 <br /> MSD Lab Sample ID: 720-31364-A-20 MSD Analysis Batch: 720-80856 Instrument ID: CHMSV2 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 10291031.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/30/2010 0010 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/30/2010 0010 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 87 94 60-140 7 20 <br /> 1,1-Dichloroethane 101 102 60-140 1 20 <br /> Dichlorodifluoromethane 82 77 38-140 7 20 <br /> Vinyl chloride 86 85 58-140 2 20 <br /> Chloroethane 88 91 51 -140 3 20 <br /> Trichlorofluoromethane 91 91 60-140 0 20 <br /> Methylene Chloride 88 90 40-140 2 20 <br /> trans-1,2-Dichloroethene 85 90 60-140 6 20 <br /> cis-1,2-Dichloroethene 120 119 60-140 0 20 <br /> Chloroform 103 102 60-140 1 20 <br /> 1,1,1-Trichloroethane 98 100 60-140 2 20 <br /> Carbon tetrachloride 95 97 60-140 2 20 <br /> 1,2-Dichloroethane 107 104 60-140 3 20 <br /> Trichloroethene 98 101 60-140 3 20 <br /> 1,2-Dichloropropane 111 111 60-140 0 20 <br /> Dichlorobromomethane 111 108 60-140 2 20 <br /> trans-1,3-Dichloropropene 107 105 60-140 2 20 <br /> cis-1,3-Dichloropropene 105 104 60-140 1 20 <br /> 1,1,2-Trichloroethane 113 111 60-140 1 20 <br /> Tetrachloroethene 102 105 60-140 2 20 <br /> Chlorodibromomethane 102 99 60-140 2 20 <br /> Chlorobenzene 101 102 60-140 1 20 <br /> Bromoform 107 109 56-140 1 20 <br /> 1,1,2,2-Tetrachloroethane 113 116 60-140 3 20 <br /> 1,3-Dichlorobenzene 108 111 60-140 3 20 <br /> 1,4-Dichlorobenzene 103 106 60-140 2 20 <br /> 1,2-Dichlorobenzene 108 109 60-140 1 20 <br /> Chloromethane 96 92 52-140 4 20 <br /> Bromomethane 87 88 23-140 1 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 80 86 60-140 7 20 <br /> TestAmerica San Francisco Page 57 of 88 <br />