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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-31395-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-80858 Preparation: 5030B <br /> MS Lab Sample ID: 720-31393-A-127 MS Analysis Batch: 720-80858 Instrument ID: HP9 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 10291028.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/29/2010 2246 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/29/2010 2246 <br /> MSD Lab Sample ID: 720-31393-A-127 MSD Analysis Batch: 720-80858 Instrument ID: HP9 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 10291029.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/29/2010 2319 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/29/2010 2319 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 100 100 60-140 0 20 <br /> 1,1-Dichloroethane 103 103 60-140 0 20 <br /> Dichlorodifluoromethane 81 77 38-140 4 20 <br /> Vinyl chloride 84 85 58-140 1 20 <br /> Chloroethane 92 93 51 -140 2 20 <br /> Trichlorofluoromethane 95 97 60-140 2 20 <br /> Methylene Chloride 99 100 40-140 0 20 <br /> trans-1,2-Dichloroethene 94 94 60-140 0 20 <br /> cis-1,2-Dichloroethene 117 118 60-140 0 20 <br /> Chloroform 103 104 60-140 1 20 <br /> 1,1,1-Trichloroethane 105 105 60-140 0 20 <br /> Carbon tetrachloride 104 104 60-140 0 20 <br /> 1,2-Dichloroethane 100 100 60-140 0 20 <br /> Trichloroethene 105 103 60-140 1 20 <br /> 1,2-Dichloropropane 107 108 60-140 1 20 <br /> Dichlorobromomethane 112 110 60-140 2 20 <br /> trans-1,3-Dichloropropene 110 111 60-140 0 20 <br /> cis-1,3-Dichloropropene 110 110 60-140 0 20 <br /> 1,1,2-Trichloroethane 106 106 60-140 0 20 <br /> Tetrachloroethene 105 105 60-140 0 20 <br /> Chlorodibromomethane 107 106 60-140 1 20 <br /> Chlorobenzene 103 102 60-140 1 20 <br /> Bromoform 109 106 56-140 2 20 <br /> 1,1,2,2-Tetrachloroethane 106 105 60-140 1 20 <br /> 1,3-Dichlorobenzene 107 107 60-140 0 20 <br /> 1,4-Dichlorobenzene 102 102 60-140 0 20 <br /> 1,2-Dichlorobenzene 105 105 60-140 0 20 <br /> Chloromethane 103 102 52-140 1 20 <br /> Bromomethane 92 92 23-140 1 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 95 96 60-140 2 20 <br /> TestAmerica San Francisco Page 62 of 88 <br />