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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-31395-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-80859 Preparation: 5030B <br /> MS Lab Sample ID: 720-31364-A-10 MS Analysis Batch: 720-80859 Instrument ID: HP12 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 10291031.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/29/2010 2253 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/29/2010 2253 <br /> MSD Lab Sample ID: 720-31364-A-10 MSD Analysis Batch: 720-80859 Instrument ID: HP12 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 10291032.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/29/2010 2324 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/29/2010 2324 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 115 116 60-140 0 20 <br /> 1,1-Dichloroethane 111 110 60-140 0 20 <br /> Dichlorodifluoromethane 95 95 38-140 1 20 <br /> Vinyl chloride 97 105 58-140 8 20 <br /> Chloroethane 96 93 51 -140 3 20 <br /> Trichlorofluoromethane 112 113 60-140 0 20 <br /> Methylene Chloride 114 115 40-140 1 20 <br /> trans-1,2-Dichloroethene 105 107 60-140 2 20 <br /> cis-1,2-Dichloroethene 120 121 60-140 1 20 <br /> Chloroform 114 113 60-140 0 20 <br /> 1,1,1-Trichloroethane 118 119 60-140 1 20 <br /> Carbon tetrachloride 124 124 60-140 1 20 <br /> 1,2-Dichloroethane 103 105 60-140 2 20 <br /> Trichloroethene 89 73 60-140 4 20 <br /> 1,2-Dichloropropane 111 111 60-140 1 20 <br /> Dichlorobromomethane 115 117 60-140 1 20 <br /> trans-1,3-Dichloropropene 119 120 60-140 1 20 <br /> cis-1,3-Dichloropropene 120 121 60-140 1 20 <br /> 1,1,2-Trichloroethane 112 114 60-140 1 20 <br /> Tetrachloroethene 131 132 60-140 1 20 <br /> Chlorodibromomethane 120 121 60-140 1 20 <br /> Chlorobenzene 105 104 60-140 1 20 <br /> Bromoform 111 115 56-140 3 20 <br /> 1,1,2,2-Tetrachloroethane 97 100 60-140 3 20 <br /> 1,3-Dichlorobenzene 108 106 60-140 1 20 <br /> 1,4-Dichlorobenzene 104 103 60-140 1 20 <br /> 1,2-Dichlorobenzene 105 104 60-140 1 20 <br /> Chloromethane 99 101 52-140 2 20 <br /> Bromomethane 98 94 23-140 4 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 129 128 60-140 1 20 <br /> TestAmerica San Francisco Page 67 of 88 <br />