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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-31395-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-80860 Preparation: 5030B <br /> MS Lab Sample ID: 720-31367-A-3 MS Analysis Batch: 720-80860 Instrument ID: HP5 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 102910028.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/29/2010 2304 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/29/2010 2304 <br /> MSD Lab Sample ID: 720-31367-A-3 MSD Analysis Batch: 720-80860 Instrument ID: HP5 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 102910029.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/29/2010 2336 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/29/2010 2336 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 102 105 60-140 3 20 <br /> 1,1-Dichloroethane 109 110 60-140 1 20 <br /> Dichlorodifluoromethane 67 66 38-140 2 20 <br /> Vinyl chloride 87 87 58-140 1 20 <br /> Chloroethane 93 93 51 -140 0 20 <br /> Trichlorofluoromethane 99 98 60-140 1 20 <br /> Methylene Chloride 103 106 40-140 2 20 <br /> trans-1,2-Dichloroethene 96 97 60-140 1 20 <br /> cis-1,2-Dichloroethene 124 126 60-140 2 20 <br /> Chloroform 111 112 60-140 1 20 <br /> 1,1,1-Trichloroethane 113 112 60-140 0 20 <br /> Carbon tetrachloride 113 113 60-140 1 20 <br /> 1,2-Dichloroethane 113 115 60-140 1 20 <br /> Trichloroethene 108 111 60-140 2 20 <br /> 1,2-Dichloropropane 110 113 60-140 2 20 <br /> Dichlorobromomethane 117 119 60-140 1 20 <br /> trans-1,3-Dichloropropene 120 123 60-140 2 20 <br /> cis-1,3-Dichloropropene 118 119 60-140 1 20 <br /> 1,1,2-Trichloroethane 115 117 60-140 2 20 <br /> Tetrachloroethene 111 112 60-140 0 20 <br /> Chlorodibromomethane 120 121 60-140 1 20 <br /> Chlorobenzene 106 107 60-140 1 20 <br /> Bromoform 108 112 56-140 4 20 <br /> 1,1,2,2-Tetrachloroethane 107 112 60-140 4 20 <br /> 1,3-Dichlorobenzene 111 113 60-140 1 20 <br /> 1,4-Dichlorobenzene 108 110 60-140 1 20 <br /> 1,2-Dichlorobenzene 110 112 60-140 2 20 <br /> Chloromethane 89 89 52-140 1 20 <br /> Bromomethane 85 87 23-140 2 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 99 100 60-140 1 20 <br /> TestAmerica San Francisco Page 72 of 88 <br />