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Quality Control Results <br /> Client: Environmental Cost Management, Inc. Job Number: 720-31395-1 <br /> Matrix Spike/ Method: 8260B/CA_LUFTMS <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-80867 Preparation: 5030B <br /> MS Lab Sample ID: 720-31433-A-8 MS Analysis Batch: 720-80867 Instrument ID: HP5 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 103010015.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/30/2010 1801 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/30/2010 1801 <br /> MSD Lab Sample ID: 720-31433-A-8 MSD Analysis Batch: 720-80867 Instrument ID: HP5 <br /> Client Matrix: Water Prep Batch: N/A Lab File ID: 103010016.D <br /> Dilution: 1.0 Initial Weight/Volume: 10 mL <br /> Date Analyzed: 10/30/2010 1834 Final Weight/Volume: 10 mL <br /> Date Prepared: 10/30/2010 1834 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> 1,1-Dichloroethene 96 98 60-140 2 20 <br /> 1,1-Dichloroethane 105 106 60-140 1 20 <br /> Dichlorodifluoromethane 84 86 38-140 3 20 <br /> Vinyl chloride 87 92 58-140 6 20 <br /> Chloroethane 89 94 51 -140 6 20 <br /> Trichlorofluoromethane 100 104 60-140 4 20 <br /> Methylene Chloride 98 98 40-140 0 20 <br /> trans-1,2-Dichloroethene 89 91 60-140 2 20 <br /> cis-1,2-Dichloroethene 122 121 60-140 0 20 <br /> Chloroform 110 109 60-140 2 20 <br /> 1,1,1-Trichloroethane 110 109 60-140 0 20 <br /> Carbon tetrachloride 111 111 60-140 0 20 <br /> 1,2-Dichloroethane 121 115 60-140 5 20 <br /> Trichloroethene 105 105 60-140 0 20 <br /> 1,2-Dichloropropane 108 107 60-140 0 20 <br /> Dichlorobromomethane 120 118 60-140 2 20 <br /> trans-1,3-Dichloropropene 125 124 60-140 1 20 <br /> cis-1,3-Dichloropropene 118 117 60-140 1 20 <br /> 1,1,2-Trichloroethane 117 115 60-140 1 20 <br /> Tetrachloroethene 109 109 60-140 0 20 <br /> Chlorodibromomethane 124 121 60-140 2 20 <br /> Chlorobenzene 103 104 60-140 1 20 <br /> Bromoform 113 112 56-140 1 20 <br /> 1,1,2,2-Tetrachloroethane 107 110 60-140 3 20 <br /> 1,3-Dichlorobenzene 108 109 60-140 1 20 <br /> 1,4-Dichlorobenzene 106 108 60-140 2 20 <br /> 1,2-Dichlorobenzene 110 111 60-140 1 20 <br /> Chloromethane 92 97 52-140 6 20 <br /> Bromomethane 85 91 23-140 6 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroethane 95 96 60-140 1 20 <br /> TestAmerica San Francisco Page 77 of 88 <br />